Preparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin

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dc.citation.epage204
dc.citation.issue2
dc.citation.spage195
dc.citation.volume14
dc.contributor.affiliationSivas Cumhuriyet University
dc.contributor.authorHepokur, Ceylan
dc.contributor.authorNursevin Öztop, H.
dc.contributor.authorSaraydin, Dursun
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2020-12-30T08:53:37Z
dc.date.available2020-12-30T08:53:37Z
dc.date.created2020-01-24
dc.date.issued2020-01-24
dc.description.abstractОдержано полімери «з молекулярними відтисками» (молекулярно імпринтовані полімери, MIП) для високоселективного розпізнавання серотоніну. Як мономери для одержання МІП використано акриламід, метакрилову кислоту та метакриламид. Проведено полімеризацію функціональних мономерів з диметакрилатом етиленгліколю, діакрилатом 1,4- бутандіолу і триметилпропантриакрилатом з серотоніном. Видалення серотоніну з MIП проводили за допомогою суміші метанол/оцтова кислота (4:1). Синтезовано неімпринтовані полімери (НІП) без серотоніну. Одержані полімери досліджено за допомогою методів Фур‘є-спектроскопії, диференційно скануючої калориметрії, термогравіметричного аналізу та скануючої електронної мікроскопії. Встановлено вплив температури, pH і концентрації на адсорбцію серотоніну. Визначено значення селективності таможливість повторного використання.
dc.description.abstractMolecularly imprinted polymers (MIPs) were prepared for highly selective recognition of serotonin. Acrylamide, methacrylic acid and methacrylamide were selected as the monomers for the production of MIPs. Functional monomers were polymerized with ethylene glycol dimethacrylate, 1,4-butanediol diacrylate, and trimethylpropane triacrylate with serotonin (MIP-EGDMA, MIP-BUT and MIP-TMT). Serotonin was removed from MIP by the mixture of methanol/acetic acid (4:1). Nonimprinted polymers (NIPs) were synthesized without serotonin (NIP-EGDMA, NIP-BUT and NIP-TMT). For the characterization of synthesized polymers FTIR, DSC, TGA, and SEM analysis were investigated. The parameters that affect the adsorption of serotonin on polymers such as temperature, pH and concentration were evaluated. The selectivity and reusability studies were also investigated.
dc.format.extent195-204
dc.format.pages10
dc.identifier.citationHepokur C. Preparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin / Ceylan Hepokur, H. Nursevin Öztop, Dursun Saraydin // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 195–204.
dc.identifier.citationenHepokur C. Preparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin / Ceylan Hepokur, H. Nursevin Öztop, Dursun Saraydin // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 195–204.
dc.identifier.doidoi.org/10.23939/chcht14.02.195
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/55800
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 2 (14), 2020
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dc.relation.referencesen[7]JeCho S., Noh H., Won M. et al., Biosens. Bioelectron., 2018, 99, 471. https://doi.org/10.1016/j.bios.2017.08.022
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dc.relation.referencesen[27] Okutucu B.,Önal S., Talanta, 2011, 87, 74. https://doi.org/10.1016/j.talanta.2011.09.043
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dc.relation.referencesen[31] Saraydin D., Karadağ E., Tr. J. Chem., 1996, 20, 234.
dc.relation.urihttps://doi.org/10.1016/j.apsusc.2018.07.142
dc.relation.urihttps://doi.org/10.1002/cbdv.200490069
dc.relation.urihttps://doi.org/10.3390/ijms9122333
dc.relation.urihttps://doi.org/10.1016/j.aca.2016.02.046
dc.relation.urihttps://doi.org/10.3390/i7050155
dc.relation.urihttps://doi.org/10.1016/j.bios.2017.08.022
dc.relation.urihttps://doi.org/10.1016/j.aca.2005.01.052
dc.relation.urihttps://doi.org/10.3176/proc.2018.2.04
dc.relation.urihttps://doi.org/10.1016/j.elecom.2017.07.007
dc.relation.urihttps://doi.org/10.1016/j.bios.2005.05.015
dc.relation.urihttps://doi.org/10.1002/pola.20186
dc.relation.urihttps://doi.org/10.1016/S0378-4347(99)00057-2
dc.relation.urihttps://doi.org/10.1016/j.aca.2007.01.016
dc.relation.urihttps://doi.org/10.1016/j.snb.2012.05.040
dc.relation.urihttps://doi.org/10.1016/j.aca.2010.04.019
dc.relation.urihttps://doi.org/10.1016/j.chroma.2006.09.065
dc.relation.urihttps://doi.org/10.1002/macp.1987.021880408
dc.relation.urihttps://doi.org/10.1016/j.talanta.2008.05.033
dc.relation.urihttps://doi.org/10.1016/S0006-3495(96)79393-1
dc.relation.urihttps://doi.org/10.1016/S1386-1425(02)00308-6
dc.relation.urihttps://doi.org/10.1021/jp109337a
dc.relation.urihttps://doi.org/10.1016/S0142-9612(99)00048-4
dc.relation.urihttps://doi.org/10.1002/pen.23950
dc.relation.urihttps://doi.org/10.1016/j.talanta.2011.09.043
dc.relation.urihttps://doi.org/10.1039/jr9600003973
dc.relation.urihttps://doi.org/10.1007/s12221-017-7215-7
dc.rights.holder© Національний університет “Львівська політехніка”, 2020
dc.rights.holder© Hepokur C., Oztop N., Saraydin D., 2020
dc.subjectакриламід
dc.subjectметакрилова кислота
dc.subjectметакриламід
dc.subjectмолекулярно-імпринтовані полімери
dc.subjectсеротонін
dc.subjectacrylamide
dc.subjectmethacrylic acid
dc.subjectmethacrylamide
dc.subjectmolecularly imprinted polymers
dc.subjectserotonin
dc.titlePreparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin
dc.title.alternativeОдержання та характеристика полімерів з “молекулярними відтисками” для селективного розпізнавання серотоніну
dc.typeArticle

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Chemistry & Chemical Technology. – 2020. – Vol. 14, No. 2