Obtaining of coumarone-indene resins based on light fraction of coal tar. 2. Coumarone-indene resins with epoxy groups

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dc.citation.epage100
dc.citation.issue1
dc.citation.spage93
dc.citation.volume12
dc.contributor.affiliationLviv Polytechnic National University
dc.contributor.affiliationGdansk University of Technology
dc.contributor.authorBratychak, Michael
dc.contributor.authorRipak, Oresta
dc.contributor.authorNamiesnik, Jacek
dc.contributor.authorShyshchak, Olena
dc.contributor.authorAstakhova, Olena
dc.coverage.placenameLviv
dc.date.accessioned2019-01-29T12:53:37Z
dc.date.available2019-01-29T12:53:37Z
dc.date.created2018-01-20
dc.date.issued2018-01-20
dc.description.abstractЗ використанням легкої фракції кам’яно- вугільної смоли та отриманої на її основі фракції, що википає за температур 423–463 К з додаванням стиролу і гліцидил- метакрилату розроблений метод одержання інден-кума- ронових смол з епоксидними групами (ІКСЕ). ІКСЕ отримані за радикальною коолігомеризацією з використанням як ініціатор монопероксидної похідної дигліцидилового етеру діоксидифе- нілпропану (ПО). Вивчена терміна стабільність ПО. Встановлено вплив кількості ініціатора, температури та тривалості реакції на вихід та температуру розм’якшення ІКСЕ. Структура синтезованих ІКСЕ підтверджена ІЧ- та 1Н ЯМРспектроскопічними дослідженнями.
dc.description.abstractCoumarone-indene resins with epoxy groups (CIRE) have been obtained using light fraction of coal tar or fraction with the distillation range of 423–463 K based on it. Styrene and glycidyl methacrylate were used as modifiers. CIRE were synthesized via radical cooligomerization using monoperoxide derivative of dioxyphenylpropane diglycidyl ether (PO) as an initiator. Thermal stability of PO has been studied. The effect of initiator amount, reaction temperature and time on the yield and softening temperature of CIRE has been determined. The structure of the synthesized CIRE was confirmed by IR and 1H NMR spectroscopy.
dc.format.extent93-100
dc.format.pages8
dc.identifier.citationObtaining of coumarone-indene resins based on light fraction of coal tar. 2. Coumarone-indene resins with epoxy groups / Michael Bratychak, Oresta Ripak, Jacek Namiesnik, Olena Shyshchak, Olena Astakhova // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2-18. — Vol 12. — No 1. — P. 93–100.
dc.identifier.citationenObtaining of coumarone-indene resins based on light fraction of coal tar. 2. Coumarone-indene resins with epoxy groups / Michael Bratychak, Oresta Ripak, Jacek Namiesnik, Olena Shyshchak, Olena Astakhova // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2-18. — Vol 12. — No 1. — P. 93–100.
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/43919
dc.language.isoen
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 1 (12), 2-18
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dc.relation.referencesen[2] BratychakM., Hetmanchuk Yu., Khimichna Technologiya Syntezu Vysokomolekuliarnykh Spoluk. Vyd-vo NULP, Lviv 2009.
dc.relation.referencesen[3] BratychakM., GaginM., Shyshchak O., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 15.
dc.relation.referencesen[4] BratychakM., GaginM., Shyshchak O., Brostow W., Chemia i Inzyneria Ekologiczna, 2004, 11, 21.
dc.relation.referencesen[5] GaginM., BratychakM., Shyshchak O., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 27.
dc.relation.referencesen[6] Skibitskiy V., Grynyshyn O., BratychakM., Brostow W., Chemia i Inzyneria Ekologiczna, 2004, 11, 41.
dc.relation.referencesen[7] BratychakM., Romashko I., Shyshchak O., WaclawekW., Ecolog. Chem. Eng., 2006, 13, 7.
dc.relation.referencesen[8] BratychakM., Shyshchak O., Romashko I., WaclawekW., Ecolog. Chem. Eng., 2006, 13, 17.
dc.relation.referencesen[9] BratychakM., Romashko I., Shyshchak O. et al., Ecolog. Chem. Eng., 2007, 14, 245.
dc.relation.referencesen[10] BratychakM., Brostow W., Pietkiewicz D., Topilnytskiy P., Chem. Chem. Technol., 2007, 1, 155.
dc.relation.referencesen[11] BratychakM., Grynyshyn O., Astakhova O. et al., Ecolog. Chem. Eng., 2008, 15, 387.
dc.relation.referencesen[12] BratychakM., Shust O., Chervinskyy T. et al., Ecolog. Chem. Eng., 2011, 18, 49.
dc.relation.referencesen[13] Chervinskyy T., BratychakM., GaginM., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 1225.
dc.relation.referencesen[14] BratychakM., Grynyshyn O., Shyshchak O. et al., Ecolog. Chem. Eng., 2007, 14, 225.
dc.relation.referencesen[15] Grynyshyn O., BratychakM., Krynytskiy V., Donchak V., Chem. Chem. Technol., 2008, 2, 47.
dc.relation.referencesen[16] BratychakM., Grynyshyn O., Astakhova O. et al., Ecolog. Chem. Eng., 2010, 17, 309.
dc.relation.referencesen[17] Tiwari H., Sharma R., Kumar R. et al., Coke Chem., 2014, 57, 477. https://doi.org/10.3103/S1068364X14120072.
dc.relation.referencesen[18] Pyshyev S., Gunka V., Grytsenko Y., BratychakM., Chem. Chem. Technol., 2016, 10, 631.https://doi.org/10.23939/chcht10.04si.631
dc.relation.referencesen[19] BratychakM., Astakhova O., Shyshchak O. et al., Chem. Chem. Technol., 2017, 11, 509.https://doi.org/10.23939/chcht11.04.509
dc.relation.referencesen[20] https://www.chemicalbook.com/ChemicalProductProperty_ EN_CB3415111.htm.
dc.relation.referencesen[21] BratychakM., Chervinskyy T., GaginM. et al., Ukr. Khim. Zh., 2005, 71, 50.
dc.relation.referencesen[22] Braun D., Cherdron H., RehahnM. et al., Polymer Synthesis: Theory and Practice: Fundamentals, Methods, Experiments, 5th edn. Springer-Verlag, Berlin Heidelberg 2013. https:/doi.org/10.1007/978-3-642-28980-4_1
dc.relation.referencesen[23] ASTM- D36/D36M - 14e1. Standard Test Method for Softening Point of Bitumen (Ring-and-Ball Apparatus).https://www.astm.org/Standards/D36.htm
dc.relation.referencesen[24] Wilson G., Henderson J., Caruso M. et al., J. Polym. Sci. A,2010, 48, 2698. https://doi.org/10.1002/pola.24053
dc.relation.urihttps://doi.org/10.3103/S1068364X14120072
dc.relation.urihttps://doi.org/10.23939/chcht10.04si.631
dc.relation.urihttps://doi.org/10.23939/chcht11.04.509
dc.relation.urihttps://www.chemicalbook.com/ChemicalProductProperty_
dc.relation.urihttps://www.astm.org/Standards/D36.htm
dc.relation.urihttps://doi.org/10.1002/pola.24053
dc.rights.holder© Національний університет „Львівська політехніка“, 2018
dc.rights.holder© Bratychak M., Ripak O., Namiesnik J., Shyshchak O., Astakhova O., 2018
dc.subjectінден-кумаронова смола
dc.subjectкам’яно- вугільна смола
dc.subjectстирол
dc.subjectмалеїновий ангідрид
dc.subjectгліцидилметакри- лат
dc.subjectпероксид
dc.subjectтермоліз
dc.subjectІЧ-спектроскопія
dc.subject1Н ЯМР- спектроскопія
dc.subjectcoumarone-indene resin
dc.subjectcoal tar
dc.subjectglycidyl methacrylate
dc.subjectstyrene
dc.subjectperoxide
dc.subjectthermolysis
dc.subjectinfrared spectroscopy
dc.subject1H NMR spectroscopy
dc.titleObtaining of coumarone-indene resins based on light fraction of coal tar. 2. Coumarone-indene resins with epoxy groups
dc.title.alternativeОдержання інден-кумаронових смол з легкої фракції кам‘яно-вугільної смоли. 2. Інден-кумаронові смоли з епоксидними групами
dc.typeArticle

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Chemistry & Chemical Technology. – 2018. – Vol. 12, No. 1