Hydrocarbon compounds and plausible mechanism of gas generation in “shale” gas prospective silurian deposits of Lviv Paleozoic depression

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dc.citation.issue1 (22)
dc.citation.journalTitleГеодинаміка : науковий журнал
dc.citation.spage26
dc.contributor.affiliationІнститут геології і геохімії горючих копалин НАН України
dc.contributor.affiliationInstitute of Geology and Geochemistry of Combustible Minerals of NAS of Ukraine
dc.contributor.affiliationИнститут геологии и геохимии горючих ископаемых НАН Украины
dc.contributor.authorНаумко, І. М.
dc.contributor.authorКуровець, І. М.
dc.contributor.authorЗубик, Н. І.
dc.contributor.authorБацевич, Н. В.
dc.contributor.authorСахно, Б. Е.
dc.contributor.authorЧепусенко, П. С.
dc.contributor.authorNaumko, I.
dc.contributor.authorKurovets’, I.
dc.contributor.authorZubyk, M.
dc.contributor.authorBatsevych, N.
dc.contributor.authorSakhno, B.
dc.contributor.authorChepusenko, P.
dc.contributor.authorНаумко, И. М.
dc.contributor.authorКуровец, И. М.
dc.contributor.authorЗубик, Н. И.
dc.contributor.authorБацевич, Н. В.
dc.contributor.authorСахно, Б. Э.
dc.contributor.authorЧепусенко, П. С.
dc.date.accessioned2018-09-12T09:08:36Z
dc.date.available2018-09-12T09:08:36Z
dc.date.created2017-06-13
dc.date.issued2017-06-13
dc.description.abstractМета. Дослідження складу газу закритої пористості (флюїдні включення у мінералах і закриті пори порід) перспективно газоносних граполітових аргілітів силуру Львівського палеозойського прогину та обґрунтування вірогідного механізму і динаміки газогенерації під час формування “сланцевого” газу у продуктивних верствах чорносланцевих формацій регіону. Методика. Склад летких сполук флюїдних включень у мінералах і закритих пор порід, їхні відносні газонасиченість і водонасиченість визначали мас-спектрометричним хімічним методом. Включення і закриті пори розкривали за допомогою розчавлювання стандартної проби (наважка 200 мг, фракція +1–2 мм) у невеликій металевій циліндричній ступці між двома плоскопаралельними твердосплавними (побєдітовими) поверхнями в умовах високого вакууму (порядка 1·10-3 Па). Результати. За даними мінералофлюїдологічних досліджень у газовій фазі флюїдних включень у мінералах і закритих пор граптолітових аргілітів силуру Львівського палеозойського прогину домінує метан (до 100 об. %) за незначних вмістів етану, діоксиду вуглецю, азоту. Відсутність пари води може свідчити про “сухість” вуглеводневмісних систем, а низькі значення відносної газонасиченості – про перетворення органічної речовини як джерела летких вуглеводневих сполук за невисоких (головно, літостатичних) тисків. Це свідчить про реальність перебігу процесів газоутворення під час трансформації органічної речовини аргілітових верств. На порядок вища відносна газонасиченість включень у кальциті, яким заліковані субвертикальні тріщини в аргілітах, і поява пари води вказує на ймовірний приплив глибинних мігрувальних флюїдів потужними тріщинними системами. Обґрунтовано вірогідний механізм і динаміку газогенерації з подальшим захопленням газу у вільному стані та сорбцією і окклюзією породами, інтенсифікований впливом глибинних флюїдів. Він основується на зіставленні даних про склад летких сполук флюїдних включень у мінералах і закритих пор перспективно газоносних аргілітів та сорбційно-генераційні процеси утворення метану у вугіллі, виходячи з принципової єдності природи перетворення розсіяної і концентрованої форм органічної речовини. Наукова новизна. Вперше у флюїдних включеннях у мінералах і закритих порах (кавернах, тріщинах) перспективних на “сланцевий” газ граптолітових аргілітів палеозою Волино-Поділля встановлено релікти відновних, практично істотно водневодневих безводних (“сухих”) флюїдів. Це вказує на наявність геофлюїдодинамічних умов, як для генерації вуглеводнів у процесах перетворення органічної речовини, сорбованих і окклюдованих мінеральною і органічною складовою порід на стадії катагенезу, так і припливу глибинних вуглеводневих флюїдів, і, отже, підтверджує газосланцевий потенціал надр регіону. Практична значущість. Оцінено вплив летких сполук закритої пористості (флюїдні включення у мінералах і закриті пори вмісних порід (граптолітових аргілітів) на сумарну потенційну газоносність сланцевовмісних верств, що матиме значення (не заторкуючи інших аспектів проблеми) за можливого підрахунку ресурсів (запасів) “сланцевого” газу.
dc.description.abstractPurpose. Investigations of composition of gas within closed porosity (fluid inclusions and closed pores in rocks) of prospective gas-bearing Silurian graptolitic argillites of Lviv Paleozoic depression and ground of plausible mechanism and dynamics of gas generation during “shale” gas formation in productive strata of blackshale formations of the region. Methodology. The composition of volatile of fluid inclusions and closed pores of rocks, and their relative gas saturation and water saturation were determined by mass spectrometric chemical method. Inclusions and closed pores were opened by crushing a standard sample (sample weight 200 mg, +1-2 mm fraction) in a small metal cylindrical mortar between two plane-parallel hard carbide alloy (pobedit) surfaces in high vacuum (approx. 1×10-3 Pa). Results. According to data for mineral-fluidological research, methane prevails (up to 100 vol.%) with minor content of ethane, carbon dioxide and nitrogen in gas phase of fluid inclusions and closed pores of Silurian graptolitic argillites of Lviv Paleozoic depression. Lack of the steam may indicate “dryness” of hydrocarbon-bearing systems, and low values of relative gas saturation – the conversion of organic matter as a source of volatile hydrocarbon compounds at the low (mainly, litostatic) pressures. This indicates the reality of passage of processes of gas production during the transformation of organic matter of argillite strata. Higher by one order the relative gas saturation of inclusions in calcite, which healed subvertical fractures in argillites, had the appearance of the steam indicates the likely influx of deep-seated migrating fluids via powerful crack systems. It was grounded that the plausible mechanism and dynamics of gas generation followed by capture of gas in free state and sorption and occlusion within rocks, intensified by influence of deepseated fluids. It is based on a comparison of data on the composition of volatile compounds of fluid inclusions and closed pores of prospective gas-bearing argillites and sorption-generation processes of methane generation in coal, based on the principle of unity of nature of transformation of dispersed and concentrated form of organic matter. Originality. For the first time relics of renewable, almost substantially hydrocarbon anhydrous (dry) fluids in fluid inclusions and closed pores (cavities, cracks) of shale gas prospective graptolitic argillites of the Paleozoic of the Volyn-Podillya there were found. This indicates the presence geo-fluid-dynamic conditions, both for the generation of hydrocarbons in the conversion of organic matter, absorbed and occluded by mineral and organic component of rocks at the stage of katagenesis, and the influx of deep-seated hydrocarbon fluids, and thus confirms shale gas potential of mineral resources of the region. Practical significance. The influence of volatile compounds in closed porosity (fluid inclusions and closed pores of host rocks (graptolitic argillites)) for the total gas-bearing potential of shale-bearing strata is estimated, which will be significant, regardless of other aspects of the problem (especially social and environmental issues), for the eventual estimate of shale gas resources (reserves).
dc.description.abstractЦель. Исследование состава газа закрытой пористости (флюидные включения в минералах и закрытые поры пород) перспективно газоносных граполитовых аргиллитов силура Львовского палео- зойского прогиба и обоснование вероятного механизма и динамики газогенерации при формировании “сланцевого” газа в продуктивных толщах черносланцевых формаций региона. Методика. Состав летучих соединений флюидных включений в минералах и закрытых пор пород, их относительные газонасыщенность и водонасыщенность определяли масс-спектрометрическим химическим методом. Включения и закрытые поры раскрывали путем раздавливания стандартной пробы (навеска 200 мг, фракция +1-2 мм) в небольшой металлической цилиндрической ступке между двумя плоскопа- раллельными твердосплавными (победитовыми) поверхностями в условиях высокого вакуума (порядка 1·10-3 Па). Результаты. По данным минералофлюидологических исследований в газовой фазе флюидных включений в минералах и закрытых пор граполитовых аргиллитов силура Львовского палеозойского прогиба доминирует метан (до 100 об. %) при незначительных содержаниях этана, диоксида углерода, азота. Отсутствие паров воды может свидетельствовать о “сухости” углеводородосодержащих систем, а низкие значения относительной газонасыщенности – о превращении органического вещества в качестве источника летучих углеводородных соединений при невысоких (приимущественно, литостатических) давлениях. Это свидетельствует о реальности прохождения процессов газообразования при транс- формации органического вещества аргиллитовых толщ. На порядок высшая относительная газона- сыщенность включений в кальците, которым залечены субвертикальные трещины в аргиллитах, и появление паров воды указывает на вероятный приток глубинных мигрирующих флюидов мощными трещинными системами. Обоснован вероятный механизм и динамика газогенерации с дальнейшим захватом газа в свободном состоянии и сорбцией и окклюзией породами, интенсифицированный влиянием глубинных флюидов. Он базируется на сопоставлении данных о составе летучих соединений флюидных включений в минералах и закрытых пор перспективно газоносных аргиллитов и сорбционно- генерационных процессах образования метана в углях, исходя из принципиального единства природы преобразования рассеянной и концентрированной форм органического вещества. Научная новизна. Впервые во флюидных включениях в минералах и закрытых порах (кавернах, трещинах) перспективных на “сланцевий” газ граптолитовых аргиллитов палеозоя Волино-Подолии выявлены реликты восста- новленных, практически существенно углеводородных безводных (“сухих”) флюидов. Это указывает на наличие геофлюидодинамических условий, как для генерации углеводородов в процессах превращения органического вещества, сорбированных и окклюдированных минеральной и органической состав- ляющими пород на стадии катагенеза, так и притока глубинных углеводородных флюидов, и, таким образом, подтверждает газосланцевый потенциал недр региона. Практическое значение. Оценено влияние летучих соединений закрытой пористости (флюидные включения в минералах и закрытые поры вмещающих пород (граптолитовых аргиллитов) на суммарную потенциальную газоносность сланце- вовмещающих толщ, что будет иметь значение (не затрагивая других аспектов проблемы) при возможном подсчете ресурсов (запасов) “сланцевого” газа.
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dc.identifier.citationHydrocarbon compounds and plausible mechanism of gas generation in “shale” gas prospective silurian deposits of Lviv Paleozoic depression / I. Naumko, I. Kurovets’, M. Zubyk, N. Batsevych, B. Sakhno, P. Chepusenko // Геодинаміка : науковий журнал. — Львів : Видавництво Львівської політехніки, 2017. — № 1 (22). — С. 26–41.
dc.identifier.citationenHydrocarbon compounds and plausible mechanism of gas generation in “shale” gas prospective silurian deposits of Lviv Paleozoic depression / I. Naumko, I. Kurovets’, M. Zubyk, N. Batsevych, B. Sakhno, P. Chepusenko // Heodynamika : naukovyi zhurnal. — Lviv : Vydavnytstvo Lvivskoi politekhniky, 2017. — No 1 (22). — P. 26–41.
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/42639
dc.language.isoen
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dc.relation.referencesenkonferencii s mezhdunarodnym uchastiem,
dc.relation.referencesenposvyaschennoj 100-letiyu so dnya rozhdeniya
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dc.relation.referencesenvuhlevodniv osadovykh baseiniv Ukrayiny
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dc.relation.referencesenuchastyu (Kyiv, 17–18 lystopada 2015 r.)
dc.relation.referencesen[Geochronology and ore prospecting of the Precambrian
dc.relation.referencesenand Fanerozoic (to the 100-anniversary
dc.relation.referencesensince the birthday of academician of the AS of
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dc.relation.referencesenverstvakh pivdenno-zakhidnoyi
dc.relation.referencesenokrayiny Skhidnoyevropeys'koyi platformy i prylehlykh
dc.relation.referencesenheostruktur (za vklyuchennyamy u mineralakh)
dc.relation.referencesen[Fluids of postsedimentogenous processes
dc.relation.referencesenwithin sedimentary and sedimentary-volcanogenous
dc.relation.referencesenstrata in South-Western margin of the East
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dc.relation.referencesenmehanizme gazogeneratsii v perspektivnyh
dc.relation.referencesenna "slantsevyiy" gaz otlozheniyah (na
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dc.relation.referencesenmechanism of gas generation in the perspective
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dc.relation.referencesengenezis, prognozy, perspektivy osvoeniia: Materialy
dc.relation.referencesenVserossiiskoj konferencii s mezhdunarodnym
dc.relation.referencesenuchastiem (Moskva, 12–14 noyabrya 2013 g.)
dc.relation.referencesen[Unconventional sources of hydrocarbons: Spreading,
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dc.relation.referencesenv mineralah perspektivno slantsevogazonosnyh
dc.relation.referencesenkompleksov palezoia Volyno-Podolii
dc.relation.referencesen(zapad Ukrainy) [First data on the composition of
dc.relation.referencesenthe volatile of fluid inclusions promising shale gas
dc.relation.referencesencomplexes of Palezoic of the Volyn-Podolia (West
dc.relation.referencesenof Ukraine)]. KhV Vserossiiskaia konferenciia po
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dc.relation.referencesenconference on thermobarogeochemistry: abstractsmaterials
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dc.relation.referencesen(na prykladi L'vivs'koho paleozois'koho
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dc.relation.referencesenzakhidnykh oblastyakh Ukrayiny [Bitumen-oil-gasgeological
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dc.relation.referencesen"Oil and gas of Ukraine–2013". For the 20th
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dc.relation.referencesenthe Lviv-Volyn Basin]. Heolohiya i heokhimiya
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dc.relation.referencesenkharakterystyka syluriis'koho vodonosnoho
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dc.relation.referencesenkonteksti problemy "slantsevoho" hazu [Hydrogeochemical
dc.relation.referencesencharacteristic of the Silurian aquifer
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dc.relation.referencesencontext of "shale" gas problem]. Heolohiya i
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dc.rights.holder© Інститут геології і геохімії горючих копалин Національної академії наук України, 2017
dc.rights.holder© Інститут геофізики ім. С. І. Субботіна Національної академії наук України, 2017
dc.rights.holder© Державна служба геодезії, картографії та кадастру України, 2017
dc.rights.holder© Львівське астрономо-геодезичне товариство, 2017
dc.rights.holder© Національний університет “Львівська політехніка”, 2017
dc.rights.holder© І. М. Наумко, І. М. Куровець, Н. І. Зубик, Н. В. Бацевич, Б. Е. Сахно, П. С.Чепусенко
dc.subjectлеткі компоненти
dc.subjectфлюїдні включення
dc.subjectзакриті пори
dc.subject“сланцевий” газ
dc.subjectграптолітові аргіліти
dc.subjectсилур
dc.subjectЛьвівський палеозойський прогин
dc.subjectvolatile
dc.subjectfluid inclusions
dc.subjectclosed pores
dc.subject“shale” gas
dc.subjectgraptolitic argillites
dc.subjectSilurian
dc.subjectLviv Paleozoic depression
dc.subjectлетучие компоненты
dc.subjectфлюидные включения
dc.subjectзакрытые поры
dc.subject“сланцевый” газ
dc.subjectграптолитовые аргиллиты
dc.subjectсилур
dc.subjectЛьвовский палеозойский прогиб
dc.subject.udc548.4
dc.subject.udc550.83
dc.subject.udc553.98
dc.subject.udc551.73 (477.8)
dc.titleHydrocarbon compounds and plausible mechanism of gas generation in “shale” gas prospective silurian deposits of Lviv Paleozoic depression
dc.title.alternativeВуглеводневі сполуки та вірогідний механізм газогенерації у перспективних на “сланцевий” газ відкладах силуру Львівського палеозойського прогину
dc.title.alternativeУглеводородные соединения и вероятный механизм газогенерации в перспективных на “сланцевый” газ отложениях силура Львовского палеозойского прогиба
dc.typeArticle

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