Optimized Design and Fabrication of Polyethylene Glycol 1000/Polyamide 6(PEG1000/PA6) Nanofibers for Phase Change Materials (PCMs) Application
| dc.citation.epage | 396 | |
| dc.citation.issue | 2 | |
| dc.citation.spage | 386 | |
| dc.contributor.affiliation | Shiraz University | |
| dc.contributor.author | Karimian, Fariba | |
| dc.contributor.author | Karimi, Gholamreza | |
| dc.contributor.author | Khorram, Mohammad | |
| dc.contributor.author | Daraeinejad, Reihaneh | |
| dc.contributor.author | Abdi, Mahnaz M. | |
| dc.coverage.placename | Львів | |
| dc.coverage.placename | Lviv | |
| dc.date.accessioned | 2024-02-12T08:30:35Z | |
| dc.date.available | 2024-02-12T08:30:35Z | |
| dc.date.created | 2023-03-16 | |
| dc.date.issued | 2023-03-16 | |
| dc.description.abstract | Ультрадисперсні нановолокна з фазовим переходом на основі поліетиленгліколю 1000 (PEG1000) як матеріалу з фазовим переходом (PCM) та поліаміду 6 (PA6) як допоміжного матеріалу виготовлено методом однонаправленого електроспінінгу на систематизованій основі, запланованій програмним забезпеченням Design-Expert®. Застосовано метод поверхневого відгуку (RSM) для оптимізації параметрів та умов, що ведуть до мінімізації діаметра волокна. За допомогою центрального композиційного плану (CCD) вивчено вплив вмісту PEG, прикладеної напруги, калібра голки та швидкості потоку на характеристики волокна. Згідно з розрахунками за квадратичною моделлю, мінімальний діаметр нановолокон становить 64,33 нм; фактичний діаметр волокон, виготовлених за оптимальних умов, показав дуже низьку відносну стандартну похибку (RSE). Встановлено, що масове співвідношення PEG/ PA6 найбільше впливає на діаметр волокон. Результати FTIR та FE-SEM підтвердили інкапсуляцію PEG у PA6, і відсутність змін у морфології після тестів на нагрівання. Для подальшого дослідження морфологічної структури та якості інкапсуляції PEG1000 у матрицях PA6 композиційні волокна оброблено розчинником з використанням етанолу. Запропоновано новий інноваційний метод контролю умов електроспінінгу для інкапсуляції матеріалів з фазовим переходом у полімерних матрицях, що дуже важливо у програмах енергозбереження/енерговідновлення. | |
| dc.description.abstract | Ultrafine phase change nanofibers based on polyethylene glycol 1000 (PEG1000) as phase change material (PCM) and polyamide 6 (PA6) as a supporting material were prepared in a systematic manner planned by the Design-Expert® software using the uniaxial electrospinning. Research surface methodology (RSM) was carried out to optimize the parameters and conditions leading to minimize the fiber diameter. The effect of PEG content, applied voltage, needle gauge, and flow rate on the fiber characteristics was studied by a central composite design (CCD). The minimum diameter of nanofibers was predicted by a quadratic model to be 64.33 nm and the actual fibers diameter prepared under optimal condition showed a very low relative standard error (RSE). It was shown that the PEG/PA6 mass ratio has the dominant effect on the fibers diameter. The results from FTIR and FE-SEM images confirmed well encapsulated PEG in PA6 and no leakage and morphology alterations were observed after heating tests. To further investigate morphological structure and the quality of PEG1000 encapsulation in PA6 matrices, the composite fibers underwent a solvent treatment using ethanol. The results proposed a new innovative method to control operational electrospinning conditions for encapsulating phase change materials in polymer matrices which is very important in thermal energy saving/retrieving applications. | |
| dc.format.extent | 386-396 | |
| dc.format.pages | 11 | |
| dc.identifier.citation | Optimized Design and Fabrication of Polyethylene Glycol 1000/Polyamide 6(PEG1000/PA6) Nanofibers for Phase Change Materials (PCMs) Application / Fariba Karimian, Gholamreza Karimi, Mohammad Khorram, Reihaneh Daraeinejad, Mahnaz M. Abdi // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2023. — Vol 17. — No 2. — P. 386–396. | |
| dc.identifier.citationen | Optimized Design and Fabrication of Polyethylene Glycol 1000/Polyamide 6(PEG1000/PA6) Nanofibers for Phase Change Materials (PCMs) Application / Fariba Karimian, Gholamreza Karimi, Mohammad Khorram, Reihaneh Daraeinejad, Mahnaz M. Abdi // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2023. — Vol 17. — No 2. — P. 386–396. | |
| dc.identifier.doi | doi.org/10.23939/chcht17.02.386 | |
| dc.identifier.issn | 1996-4196 | |
| dc.identifier.uri | https://ena.lpnu.ua/handle/ntb/61242 | |
| dc.language.iso | en | |
| dc.publisher | Видавництво Львівської політехніки | |
| dc.publisher | Lviv Politechnic Publishing House | |
| dc.relation.ispartof | Chemistry & Chemical Technology, 2 (17), 2023 | |
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| dc.rights.holder | © Національний університет “Львівська політехніка”, 2023 | |
| dc.rights.holder | © Karimian F., Karimi G., Khorram M., Daraeinejad R., Abdi M., 2023 | |
| dc.subject | електроспінінг | |
| dc.subject | матеріал з фазовим переходом (PCM) | |
| dc.subject | метод поверхневого відгуку (RSM) | |
| dc.subject | поліетиленгліколь | |
| dc.subject | поліамід 6 | |
| dc.subject | electrospinning | |
| dc.subject | phase change material (PCM) | |
| dc.subject | response surface methodology (RSM) | |
| dc.subject | polyethylene glycol | |
| dc.subject | polyamide 6 | |
| dc.title | Optimized Design and Fabrication of Polyethylene Glycol 1000/Polyamide 6(PEG1000/PA6) Nanofibers for Phase Change Materials (PCMs) Application | |
| dc.title.alternative | Оптимізований дизайн та одержання поліетиленгліколь 1000/поліамід 6 (PEG1000/PA6) нановолокон як матеріалів з фазовим переходом (PCMS) | |
| dc.type | Article |
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