The Immobilized Cu-Ni-Fe-Cr Layered Double Hydroxide on Silica-Layered Magnetite as a Reusable Mesoporous Catalyst for Convenient Conversion of Epoxides to 1,2-Diacetates

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dc.citation.epage286
dc.citation.issue2
dc.citation.spage279
dc.contributor.affiliationUrmia University
dc.contributor.authorZeynizadeh, Behzad
dc.contributor.authorGilanizadeh, Masumeh
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2024-02-12T08:30:44Z
dc.date.available2024-02-12T08:30:44Z
dc.date.created2023-03-16
dc.date.issued2023-03-16
dc.description.abstractДосліджено шаруватий подвійний гідроксид Cu-Ni-Fe-Cr (LDH), іммобілізований на шарі магнетиту (Fe3O4@SiO2@Cu-Ni-Fe-Cr LDH) для розкриття кільця різних епоксидів оцтовим ангідридом з метою отримання віц-діацетатів протягом 15–40 хв із високим виходом. Багаторазове використання нано-LDH також вивчали протягом шести послідовних циклів без значних втрат каталітичної активності.
dc.description.abstractIn this study, Cu-Ni-Fe-Cr layered double hydroxide (LDH) immobilized on silica layered magnetite (Fe3O4@SiO2@Cu-Ni-Fe-Cr LDH) was investigated towards ring opening of diverse epoxides with acetic anhydride to afford vic-diacetates within 15–40 min in high yields. Reusability of the nano-LDH was also studied for 6 consecutive cycles without the significant loss of catalytic activity.
dc.format.extent279-286
dc.format.pages8
dc.identifier.citationZeynizadeh B. The Immobilized Cu-Ni-Fe-Cr Layered Double Hydroxide on Silica-Layered Magnetite as a Reusable Mesoporous Catalyst for Convenient Conversion of Epoxides to 1,2-Diacetates / Behzad Zeynizadeh, Masumeh Gilanizadeh // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2023. — Vol 17. — No 2. — P. 279–286.
dc.identifier.citationenZeynizadeh B. The Immobilized Cu-Ni-Fe-Cr Layered Double Hydroxide on Silica-Layered Magnetite as a Reusable Mesoporous Catalyst for Convenient Conversion of Epoxides to 1,2-Diacetates / Behzad Zeynizadeh, Masumeh Gilanizadeh // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2023. — Vol 17. — No 2. — P. 279–286.
dc.identifier.doidoi.org/10.23939/chcht17.02.279
dc.identifier.issn1996-4196
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/61256
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 2 (17), 2023
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dc.relation.referencesen[1] Zeynizadeh, B.; Gilanizadeh, M. Green and Highly Efficient Approach for the Reductive Coupling of Nitroarenes to Azoxya-renes Using the New Mesoporous Fe3O4@SiO2@Co–Zr–Sb Cata-lyst. Res. Chem. Intermed. 2020, 46, 2969-2984. https://doi.org/10.1007/s11164-020-04126-7
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dc.relation.referencesen[3] Gilanizadeh, M.; Zeynizadeh, B. Synthesis and Characterization of the Immobilized Ni–Zn–Fe Layered Double Hydroxide (LDH) on Silica-Coated Magnetite as a Mesoporous and Magnetically Reusable Catalyst for the Preparation of Benzylidenemalononitriles and Bisdimedones (Tetraketones) under Green Conditions. New J. Chem. 2018, 42, 8553-8566. https://doi.org/10.1039/P.8NJ00788H
dc.relation.referencesen[4] Gilanizadeh, M.; Zeynizadeh, B. Binary Copper and Iron Oxides Immobilized on Silica-Layered Magnetite as a New Reusable Heterogeneous Nanostructure Catalyst for the Knoevenagel Condensation in Water. Res. Chem. Intermed. 2018, 44, 6053-6070. https://doi.org/10.1007/s11164-018-3475-0
dc.relation.referencesen[5] Gilanizadeh, M.; Zeynizadeh, B.; Gholamiyan E. Green Formy-lation of Alcohols Catalyzed by Magnetic Nanoparticles of the Core–Shell Fe3O4@SiO2-SO3H. Iran. J. Sci. Technol. T. A Sci. 2019, 43, 819-827. https://doi.org/10.1007/s40995-018-0594-9
dc.relation.referencesen[6] Zeynizadeh, B.; Gholamiyan, E.; Gilanizadeh, M. Magnetically Recoverable CuFe2O4 Nanoparticles as an Efficient Heterogeneous Catalyst for Green Formylation of Alcohols. Curr. Chem. Lett. 2018, 7, 121-130.
dc.relation.referencesen[7] Gilanizadeh, M.; Zeynizadeh, B. Cascade Synthesis of Fused Polycyclic Dihydropyridines by Ni–Zn–Fe Hydrotalcite (HT) Im-mobilized on Silica-coated Magnetite as Magnetically Reusable Nanocatalyst. Res. Chem. Intermed. 2019, 45, 2811-2825. https://doi.org/10.1007/s11164-019-03764-w
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dc.relation.referencesen[9] Mandal, S.; Mayadevi, S. Adsorption of Fluoride Ions by Zn–Al Layered Double Hydroxides. Appl. Clay Sci. 2008, 40, 54-62. https://doi.org/10.1016/j.clay.2007.07.004
dc.relation.referencesen[10] Goh, K.-H.; Lim, T.-T.; Dong, Z. Application of Layered Double Hydroxides for Removal of Oxyanions: A Review. Water Res. 2008, 42, 1343-1368. https://doi.org/10.1016/j.watres.2007.10.043
dc.relation.referencesen[11] Lee, W.F.; Chen, Y.-C. Effect of Hydrotalcite on the Physical Properties and Drug-release Behavior of Nanocomposite Hydrogels Based on Poly[acrylic Acid-co-poly(ethylene glycol) Methyl ETher Acrylate] Gels. J. Appl. Polym. Sci. 2004, 94, 692-699. https://doi.org/10.1002/app.20936
dc.relation.referencesen[12] Evans, D.G.; Duan, X. Preparation of Layered Double Hydroxides and their Applications as Additives in Polymers, as Precursors to Magnetic Materials and in Biology and Medicine. ChemComm 2006, 485-496 https://doi.org/10.1039/B510313B
dc.relation.referencesen[13] Chang, Y.-C.; Chang, S.-W.; Chen, D.-H. Magnetic Chitosan Nanoparticles: Studies on Chitosan Binding and Adsorption of Co(II) Ions. React. Funct. Polym. 2006, 66, 335-341. https://doi.org/10.1016/j.reactfunctpolym.2005.08.006
dc.relation.referencesen[14] Abu-Reziq, R.; Alper, H.; Wang, D.; Post, M.L. Metal Supported on Dendronized Magnetic Nanoparticles:  Highly Selective Hydroformylation Catalysts. J. Am. Chem. Soc. 2006, 128, 5279-5282. https://doi.org/10.1021/ja060140u
dc.relation.referencesen[15] Zhang, D.-H.; Li, G.-D.; Li, J.-H.; Chen, J.-S. One-Pot Synthesis of Ag-Fe3O4 Nanocomposite: A Magnetically Recyclable and Efficient Catalyst for Epoxidation of Styrene. ChemComm 2008, 29, 3414-3416. https://doi.org/10.1039/B805737K
dc.relation.referencesen[16] Gawande, M.B.; Branco, P.S.; Varma, R.S. Nano-Magnetite (Fe3O4) as a Support for Recyclable Catalysts in the Development of Sustainable Methodologies. Chem. Soc. Rev. 2013, 42, 3371-3393. https://doi.org/10.1039/P.3CS35480F
dc.relation.referencesen[17] Shylesh, S.; Schünemann, V.; Thiel, W.R. Magnetically Sepa-rable Nanocatalysts: Bridges between Homogeneous and Heteroge-neous Catalysis. Angew. Chem. Int. Ed. 2010, 49, 3428-3459. https://doi.org/10.1002/anie.200905684
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dc.relation.referencesen[26] Zeynizadeh, B.; Gilanizadeh, M.; Mohammad Aminzadeh, F. A highly Efficient Protocol for Regioselective Ring-Opening of Epoxides with Alcohols, Water, Acetic Acid, and Acetic Anhydride Catalyzed by SbF3. Phosphorus, Sulfur Silicon Relat. Elem. 2016, 191, 1051-1056. https://doi.org/10.1080/10426507.2015.1135439
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dc.relation.referencesen[28] Gilanizadeh, M.; Zeynizadeh, B. Direct Transformation of Epoxides to 1,2-Diacetates with Ac2O/B(OH)3 System. J. Chem. Soc. Pak. 2015, 37, 1234-1238.
dc.relation.referencesen[29] Das, B.; Saidi Reddy, V.; Tehseen, F. A Mild, Rapid and Highly Regioselective Ring-Opening of Epoxides and Aziridines with Acetic Anhydride under Solvent-Free Conditions Using Ammonium-12-molybdophosphate. Tetrahedron Lett. 2006, 47, 6865-6868. https://doi.org/10.1016/j.tetlet.2006.07.055
dc.relation.referencesen[30] Gilanizadeh, M.; Zeynizadeh, B. Facile Conversion of Epox-ides to 1,2-Diacetates with NAOAC 3H2O/AC2O System. Iran. J. Chem. Chem. Eng. 2016, 35, 25-29.
dc.relation.referencesen[31] Fogassy, G.; Pinel, C.; Gelbard, G. Solvent-Free Ring Opening Reaction of Epoxides Using Quaternary Ammonium Salts as Catalyst. Catal. Commun. 2009, 10, 557-560. https://doi.org/10.1016/j.catcom.2008.10.039
dc.relation.referencesen[32] Fan, R.-H.; Hou, X.-L. Tributylphosphine-Catalyzed Ring-Opening Reaction of Epoxides and Aziridines with Acetic Anhydride. Tetrahedron Lett. 2003, 44, 4411-4413. https://doi.org/10.1016/S0040-4039(03)00943-2
dc.relation.referencesen[33] Dalpozzo, R.; De Nino, A.; Nardi, M.; Russo, B.; Procopio, A. 1,2-Diacetates by Epoxide Ring Opening Promoted by Erbium(III) Triflate. ARKIVOC 2006, vi, 67-73.
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dc.rights.holder© Національний університет “Львівська політехніка”, 2023
dc.rights.holder© Zeynizadeh B., Gilanizadeh M., 2023
dc.subjectAc2O
dc.subject1
dc.subject2-діацетат
dc.subjectепоксид
dc.subjectFe3O4@SiO2@Cu-Ni-Fe-Cr LDH
dc.subjectрозкриття кільця
dc.subjectAc2O
dc.subject1
dc.subject2-diacetate
dc.subjectepoxide
dc.subjectFe3O4@SiO2@Cu-Ni-Fe-Cr LDH
dc.subjectring-opening
dc.titleThe Immobilized Cu-Ni-Fe-Cr Layered Double Hydroxide on Silica-Layered Magnetite as a Reusable Mesoporous Catalyst for Convenient Conversion of Epoxides to 1,2-Diacetates
dc.title.alternativeШаруватий подвійний гідроксид Cu-Ni-Fe-Cr, іммобілізований на магнетиті з шаром кремнію, як багаторазовий мезопористий каталізатор для практичного перетворення епоксидів в 1,2-діацетати
dc.typeArticle

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Chemistry & Chemical Technology. – 2023. – Vol. 17, No. 2