Optimization of Isocratic Ion Chromatography Methods for Simultaneous Inorganic Anions and Carboxylic Acids Determination

Simple item page
dc.citation.epage366
dc.citation.issue3
dc.citation.spage359
dc.contributor.affiliationInstitute of Environmental Engineering, Polish Academy of Sciences
dc.contributor.authorPecyna-Utylska, Paulina
dc.contributor.authorMichalski, Rajmund
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2024-01-22T12:00:12Z
dc.date.available2024-01-22T12:00:12Z
dc.date.created2022-03-16
dc.date.issued2022-03-16
dc.description.abstractПеревірено можливість кількісного окиснення альдегідів до карбонових кислот та їх визначення методом ізократної йонної хроматографії з кондуктометричним детектором. З використанням хроматографії розроблена і перевірена методологія одночасного розділення неорганічних аніонів (F-, Cl-, NO2-, Br-, NO3-, PO43-, SO42-) та карбонових кислот (форміат, ацетат та оксалат). Проведені випробовування шести аніонообмінних колонок. Встановлено, що найкращі результати отримані для колонки Dionex IonPac AS10 з 50мМ елюентом NaOH і швидкістю потоку 1,0 мл∙хв-1.
dc.description.abstractAs a part of preliminary studies, the possibility of quantitative oxidation of aldehydes to carboxylic acids and their determination by isocratic ion chromatography with conductometric detection has been tested. A methodology for the simultaneous separation of inorganic anions (F-, Cl-, NO2-, Br-, NO3-, PO43-, SO42-) and carboxylic acids (formate, acetate and oxalate) by using isocratic ion chromatography with conductivity detection have been developed and validated. Six anion-exchange columns were tested. The best results were achieved for Dionex IonPac AS10 column with 50mM NaOH eluent and flow rate of 1.0 mL∙min-1.
dc.format.extent359-366
dc.format.pages8
dc.identifier.citationPecyna-Utylska P. Optimization of Isocratic Ion Chromatography Methods for Simultaneous Inorganic Anions and Carboxylic Acids Determination / Paulina Pecyna-Utylska, Rajmund Michalski // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2022. — Vol 16. — No 3. — P. 359–366.
dc.identifier.citationenPecyna-Utylska P. Optimization of Isocratic Ion Chromatography Methods for Simultaneous Inorganic Anions and Carboxylic Acids Determination / Paulina Pecyna-Utylska, Rajmund Michalski // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2022. — Vol 16. — No 3. — P. 359–366.
dc.identifier.doidoi.org/10.23939/chcht16.03.359
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/60999
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 3 (16), 2022
dc.relation.references[1] Badea, G.; Radu, G. Introductory Chapter. In Carboxylic Acid: Key Role in Life Sciences; Badea, G.; Radu, G., Eds.; IntechOpen: London, 2018; pp 1-5.
dc.relation.references[2] Chebbi, A.; Carlier, P. Carboxylic Acids in the Troposphere, Occurrence, Sources, and Sinks: A Review. Atmos. Environ. 1996, 30, 4233-4249. https://doi.org/10.1016/1352-2310(96)00102-1
dc.relation.references[3] Niu, Y.; Li, X.; Pu, J.; Huang, Z. Organic Acids Contribute to Rainwater Acidity at a Rural Site in Eastern China. Air Qual. Atmos. Health 2018, 11, 459-469. https://doi.org/10.1007/s11869-018-0553-9
dc.relation.references[4] Craston, D.H.; Saeed, M. Analysis of Carboxylic and Related Acids in the Environment by Capillary Electrophoretic Techniques. J. Chromatogr. A 1998, 827, 1-12. https://doi.org/10.1016/S0021-9673(98)00750-X
dc.relation.references[5] Weiss, J. Handbook of Ion Chromatography; John Wiley & Sons: Hoboken, 2016.
dc.relation.references[6] Paull, B.; Michalski, R. Ion Exchange: Ion Chromatography Principles and Applications. In Encyclopedia of Analytical Science; Worsfold, P.; Poole, C.; Townshend, A.; Miró, M., Eds.; Elsevier Ltd, 2019; pp 178-189.
dc.relation.references[7] Michalski, R. Ion Chromatography as a Reference Method for Determination of Inorganic Ions in Water and Wastewater. Crit. Rev. Anal. Chem. 2006, 36, 107-127. https://doi.org/10.1080/10408340600713678
dc.relation.references[8] Michalski, R. Ion Chromatography Applications in Wastewater Analysis. Separations 2018, 5, 16. https://doi.org/10.3390/separations5010016
dc.relation.references[9] Michalski, R. Food Analysis: Ion chromatography. In Encyclopedia of Chromatography; Cazes, J., Ed.; CRC Press: Boca Raton, 2010; pp 909-913.
dc.relation.references[10] Matysiak, I.; Balcerzak, M.; Michalski, R. Ion Chromatography with Conductometric Detection for Quantitation of Formic Acid in Polish Bee Honey. J. Food Compos. Anal. 2018, 73, 55-59. https://doi.org/10.1016/j.jfca.2018.07.005
dc.relation.references[11] Michalski, R. Application of Ion Chromatography in Clinical Studies and Pharmaceutical Industry. Mini Rev. Med. Chem. 2014, 14, 862-872.
dc.relation.references[12] Michalski, R.; Błażewicz, A.; Kończyk, J.; Krupa, K.; Niziński, P. Ion Chromatography for Small Molecule Determination in Clinical and Pharmaceutical Studies. LCGC Europe 2019, 32, 629-634.
dc.relation.references[13] Tanaka, S.; Iguchi, M.; Yamanaka, K.; Yamada, T.; Nakao, N.; Yoshikazu Hashimoto, Y. Measurement of Formic Acid, Acetic Acid, Formaldehyde and Acetaldehyde in the Atmosphere by Ion Chromatography. Bunseki Kagaku 1987, 36, 12-17. https://doi.org/10.2116/bunsekikagaku.36.12
dc.relation.referencesen[1] Badea, G.; Radu, G. Introductory Chapter. In Carboxylic Acid: Key Role in Life Sciences; Badea, G.; Radu, G., Eds.; IntechOpen: London, 2018; pp 1-5.
dc.relation.referencesen[2] Chebbi, A.; Carlier, P. Carboxylic Acids in the Troposphere, Occurrence, Sources, and Sinks: A Review. Atmos. Environ. 1996, 30, 4233-4249. https://doi.org/10.1016/1352-2310(96)00102-1
dc.relation.referencesen[3] Niu, Y.; Li, X.; Pu, J.; Huang, Z. Organic Acids Contribute to Rainwater Acidity at a Rural Site in Eastern China. Air Qual. Atmos. Health 2018, 11, 459-469. https://doi.org/10.1007/s11869-018-0553-9
dc.relation.referencesen[4] Craston, D.H.; Saeed, M. Analysis of Carboxylic and Related Acids in the Environment by Capillary Electrophoretic Techniques. J. Chromatogr. A 1998, 827, 1-12. https://doi.org/10.1016/S0021-9673(98)00750-X
dc.relation.referencesen[5] Weiss, J. Handbook of Ion Chromatography; John Wiley & Sons: Hoboken, 2016.
dc.relation.referencesen[6] Paull, B.; Michalski, R. Ion Exchange: Ion Chromatography Principles and Applications. In Encyclopedia of Analytical Science; Worsfold, P.; Poole, C.; Townshend, A.; Miró, M., Eds.; Elsevier Ltd, 2019; pp 178-189.
dc.relation.referencesen[7] Michalski, R. Ion Chromatography as a Reference Method for Determination of Inorganic Ions in Water and Wastewater. Crit. Rev. Anal. Chem. 2006, 36, 107-127. https://doi.org/10.1080/10408340600713678
dc.relation.referencesen[8] Michalski, R. Ion Chromatography Applications in Wastewater Analysis. Separations 2018, 5, 16. https://doi.org/10.3390/separations5010016
dc.relation.referencesen[9] Michalski, R. Food Analysis: Ion chromatography. In Encyclopedia of Chromatography; Cazes, J., Ed.; CRC Press: Boca Raton, 2010; pp 909-913.
dc.relation.referencesen[10] Matysiak, I.; Balcerzak, M.; Michalski, R. Ion Chromatography with Conductometric Detection for Quantitation of Formic Acid in Polish Bee Honey. J. Food Compos. Anal. 2018, 73, 55-59. https://doi.org/10.1016/j.jfca.2018.07.005
dc.relation.referencesen[11] Michalski, R. Application of Ion Chromatography in Clinical Studies and Pharmaceutical Industry. Mini Rev. Med. Chem. 2014, 14, 862-872.
dc.relation.referencesen[12] Michalski, R.; Błażewicz, A.; Kończyk, J.; Krupa, K.; Niziński, P. Ion Chromatography for Small Molecule Determination in Clinical and Pharmaceutical Studies. LCGC Europe 2019, 32, 629-634.
dc.relation.referencesen[13] Tanaka, S.; Iguchi, M.; Yamanaka, K.; Yamada, T.; Nakao, N.; Yoshikazu Hashimoto, Y. Measurement of Formic Acid, Acetic Acid, Formaldehyde and Acetaldehyde in the Atmosphere by Ion Chromatography. Bunseki Kagaku 1987, 36, 12-17. https://doi.org/10.2116/bunsekikagaku.36.12
dc.relation.urihttps://doi.org/10.1016/1352-2310(96)00102-1
dc.relation.urihttps://doi.org/10.1007/s11869-018-0553-9
dc.relation.urihttps://doi.org/10.1016/S0021-9673(98)00750-X
dc.relation.urihttps://doi.org/10.1080/10408340600713678
dc.relation.urihttps://doi.org/10.3390/separations5010016
dc.relation.urihttps://doi.org/10.1016/j.jfca.2018.07.005
dc.relation.urihttps://doi.org/10.2116/bunsekikagaku.36.12
dc.rights.holder© Національний університет “Львівська політехніка”, 2022
dc.rights.holder© Pecyna-Utylska P., Michalski R., 2022
dc.subjectаніони
dc.subjectйонна хроматографія
dc.subjectвалідація
dc.subjectоптимізація
dc.subjectanions
dc.subjection chromatography
dc.subjectvalidation
dc.subjectoptimization
dc.titleOptimization of Isocratic Ion Chromatography Methods for Simultaneous Inorganic Anions and Carboxylic Acids Determination
dc.title.alternativeОптимізація методів ізократної йонної хроматографії для одночасного визначення неорганічних аніонів і карбонової кислоти
dc.typeArticle

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Chemistry & Chemical Technology. – 2022. – Vol. 16, No. 3