Development of a Needle Trap Device Packed with HKUST-1 Sorbent for Sampling and Analysis of BTEX in Air

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dc.citation.epage327
dc.citation.issue2
dc.citation.spage314
dc.contributor.affiliationHamadan University of Medical Sciences
dc.contributor.affiliationBu-Ali-Sina University
dc.contributor.authorSoury, Shiva
dc.contributor.authorBahrami, Abdulrahman
dc.contributor.authorAlizadeh, Saber
dc.contributor.authorShahna, Farshid Ghorbani
dc.contributor.authorNematollahi, Davood
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2024-01-22T11:13:01Z
dc.date.available2024-01-22T11:13:01Z
dc.date.created2022-03-16
dc.date.issued2022-03-16
dc.description.abstractВперше розроблений пристрій для утримування голки (NTD) з сорбентом HKUST-1 (металоорганічний каркас на основі Cu), який призначений для відбору проб та аналізу бензену, толуену, етилбензену та ксилену (BTEX) в атмосферному повітрі. Синтезований за допомогою електрохімічного процесу адсорбент HKUST-1 розташований у голці 22 розміру. Для забезпечення різних концентрацій BTEX шприцева помпа підключена до скляної камери для впорскування сполук BTEX з певною швидкістю. Для оптимізації аналітичних параметрів, а саме об’єму проскоку, умов десорбції та умов відбору проб використано програмне забезпечення Design-expert (версія 7). Визначено, що оптимальні умови десорбції досягаються за 548 K протягом 6 хв, а найкращі умови відбору проб – за 309 K та 20% вологості. Визначено, що показники LOQ та LOD розробленого пристрою знаходяться в межах 0,52–1,41 та 0,16–0,5 мг/м3, відповідно, а повторюваність та відтворюваність методу становлять 5,5–13,2 та 5,3–12,3 %, відповідно. Встановлено, що NTD, які зберігаються в холодильнику (> 277 K), і за кімнатної температури (298 K), зберігають проби BTEX щонайменше протягом 10 та 6 днів відповідно. Показано, що NTD з сорбентом HKUST-1 може бути використаний як надійний та корисний метод для визначення BTEX у повітрі.
dc.description.abstractIn this study, we developed a needle trap device packed with HKUST-1 (Cu-based metal-organic framework) for the sampling and analysis of benzene, toluene, ethylbenzene, and xylene (BTEX) in ambient air for the first time. The HKUST-1 was synthesized via the electrochemical process. Afterwards, the adsorbent was packed into 22 gauge needles. To provide the different concentrations of BTEX, the syringe pump was connected to the glass chamber to inject a specific rate of the BTEX compounds. Design-expert software (version 7) was used to optimize the analytical parameters including breakthrough volume, desorption conditions and sampling conditions. The best desorption conditions were achieved at 548 K for 6 min, and the best sampling conditions were determined at 309 K of sampling temperature and 20 % of relative humidity. According to the results, the limit of quantification (LOQ) and limit of detection (LOD) of the developed needle trap device (NTD) were in the range of 0.52–1.41 and 0.16–0.5 mg/m3, respectively. In addition, the repeatability and reproducibility of the method were calculated to be in the range of 5.5–13.2 and 5.3–12.3 %, respectively. The analysis of needles stored in the refrigerator (>277 K) and room temperature (298 K) showed that the NTD can store the BTEX analytes for at least 10 and 6 days, respectively. Our findings indicated that the NTD packed with HKUST-1 sorbent can be used as a trustworthy and useful technique for the determination of BTEX in air.
dc.format.extent314-327
dc.format.pages14
dc.identifier.citationDevelopment of a Needle Trap Device Packed with HKUST-1 Sorbent for Sampling and Analysis of BTEX in Air / Shiva Soury, Abdulrahman Bahrami, Saber Alizadeh, Farshid Ghorbani Shahna, Davood Nematollahi // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2022. — Vol 16. — No 2. — P. 314–327.
dc.identifier.citationenDevelopment of a Needle Trap Device Packed with HKUST-1 Sorbent for Sampling and Analysis of BTEX in Air / Shiva Soury, Abdulrahman Bahrami, Saber Alizadeh, Farshid Ghorbani Shahna, Davood Nematollahi // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2022. — Vol 16. — No 2. — P. 314–327.
dc.identifier.doidoi.org/10.23939/chcht16.02.314
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/60972
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 2 (16), 2022
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dc.relation.referencesen[1] Durmusoglu, E.; Taspinar, F.; Karademir, A. Health Risk Assessment of BTEX Emissions in the Landfill Environment. J. Hazard. Mater. 2010, 176, 870-877. https://doi.org/10.1016/j.jhazmat.2009.11.117
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dc.relation.referencesen[3] Riboni, N.; Trzcinski, J.W.; Bianchi, F.; Massera, C.; Pinalli, R.; Sidisky, L.; Dalcanale, E.; Careri, M. Conformationally Blocked Quinoxaline Cavitand as Solid-Phase Microextraction Coating for the Selective Detection of BTEX in Air. Anal. Chim. Acta 2016, 905, 79-84. https://doi.org/10.1016/j.aca.2015.12.005
dc.relation.referencesen[4] Ma J-Q., Liu L., Wang X.; Chen, L.-Z.; Lin, J.-M.; Zhao, R.-S. Development of Dispersive Solid-Phase Extraction with Polyphenylene Conjugated Microporous Polymers for Sensitive Determination of Phenoxycarboxylic Acids in Environmental Water Samples. J. Hazard. Mater. 2019, 371, 433-439. https://doi.org/10.1016/j.jhazmat.2019.03.033
dc.relation.referencesen[5] Wang, R.; Ma, X.; Zhang, X.; Li, X.; Li, D.; Dang, Y. P.8-Modified Magnetic Graphene Oxide Based Solid-Phase Extraction Coupled with Dispersive Liquid-Liquid Microextraction for Detection of Trace Phthalate Acid Esters in Water Samples. Ecotox. Environ. Safe. 2019, 170, 789-795. https://doi.org/10.1016/j.ecoenv.2018.12.051
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dc.relation.referencesen[9] Chen, J.; Zhang, B.; Zheng, D.; Dang, X.; Ai, Y.; Chen, H. A Novel Needle Trap Device Coupled with Gas Chromatography for Determination of Five Fatty Alcohols in Tea Samples. Anal. Methods 2018, 10, 5783-5789. https://doi.org/10.1039/P.8AY01894D
dc.relation.referencesen[10] Kleeblatt, J.; Schubert, J.K.; Zimmermann, R. Detection of Gaseous Compounds by Needle Trap Sampling and Direct Thermal-Desorption Photoionization Mass Spectrometry: Concept and Demonstrative Application to Breath Gas Analysis. Anal. Chem. 2015, 87, 1773-1781. https://doi.org/10.1021/ac5039829
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dc.relation.referencesen[19] Alizadeh, S.; Nematollahi, D. Convergent and Divergent Paired Electrodeposition of Metal-Organic Framework Thin Films. Sci. Rep. 2019, 9, 14325. https://doi.org/10.1038/s41598-019-50390-y
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dc.relation.referencesen[27] Witek-Krowiak, A.; Chojnacka, K.; Podstawczyk, D.; Dawiec, A.; Pokomeda, K. Application of Response Surface Methodology and Artificial Neural Network Methods in Modelling and optimization of Biosorption Process. Biores. Technol. 2014, 160, 150-160. https://doi.org/10.1016/j.biortech.2014.01.021
dc.relation.referencesen[28] Soury, S.; Bahrami, A.; Alizadeh, S.; Ghorbani-Shahna, F.; Nematollahi, D. Development of a Needle Trap Device Packed with Zinc Based Metal-Organic Framework Sorbent for the Sampling and Analysis of Polycyclic Aromatic Hydrocarbons in the Air. Microchem. J. 2019, 148, 346-354. https://doi.org/10.1016/j.microc.2019.05.019
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dc.rights.holder© Національний університет “Львівська політехніка”, 2022
dc.rights.holder© Soury S., Bahrami A., Alizadeh S., Shahna F. G., Nematollahi D., 2022
dc.subjectповітря
dc.subjectHKUST-1
dc.subjectметалоорганічний каркас
dc.subjectелектрохімія
dc.subjectпристрій для утримування голки
dc.subjectлеткі органічні сполуки
dc.subjectair
dc.subjectHKUST-1
dc.subjectmetal-organic framework
dc.subjectelectrochemical
dc.subjectneedle trap device
dc.subjectvolatile organic compounds
dc.titleDevelopment of a Needle Trap Device Packed with HKUST-1 Sorbent for Sampling and Analysis of BTEX in Air
dc.title.alternativeРозроблення пристрою для утримування голки з сорбентом HKUST-1 для відбору проб і аналізу BTEX в повітрі
dc.typeArticle

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Chemistry & Chemical Technology. – 2022. – Vol. 16, No. 2