Obtaining of coumarone-indene resins based on light fraction of coal tar 3. Coumarone-indene resins with methacrylic fragments

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dc.citation.epage385
dc.citation.issue3
dc.citation.journalTitleChemistry & Chemical Technology
dc.citation.spage379
dc.citation.volume12
dc.contributor.affiliationLviv Polytechnic National University
dc.contributor.affiliationGdansk University of Technology,Poland
dc.contributor.affiliationUniversity of Bialystok, Poland
dc.contributor.authorBratychak, Michael
dc.contributor.authorAstakhova, Olena
dc.contributor.authorPrysiazhnyi, Yuriy
dc.contributor.authorShved, Mariia
dc.contributor.authorShyshchak, Olena
dc.contributor.authorNamiesnik, Jacek
dc.contributor.authorPlonska-Brzezinska, Marta
dc.coverage.placenameLviv
dc.date.accessioned2019-06-20T11:19:22Z
dc.date.available2019-06-20T11:19:22Z
dc.date.created2018-01-20
dc.date.issued2018-01-20
dc.description.abstractЗ використанням легкої фракції кам’яно- вугільної смоли та отриманої на її основі фракції, що википає за температур 423-463 К, з додаванням метилметакрилатy розроблено метод одержання інден-кумаронових смол з метакрилатними фрагментами (CIRM). CIRM отримано за радикальною коолігомеризацією з використанням як ініціатор 2,2’-азобіс(2-метил-пропіонітрилу). Встановлено вплив кіль- кості ініціатора, температури та тривалості реакції на вихід, температуру розм’якшення та молекулярну масу CIRM. Структуру синтезованих CIRM підтверджено ІЧ– та ЯМР- спектроскопічними дослідженнями. Запропоновано використо- вувати CIRM як полімерну складову бітум-полімерних сумішей (БПС). Вивчено вплив кількості CIRM, температури та тривалості на основні характеристики БПС.
dc.description.abstractThe method for obtaining coumarone-indene resins with methacrylic fragments (CIRM) was developed with the addition of methyl methacrylate, using a light fraction of coal tar and its fraction boiling within 423– 463 К. CIRM was obtained via radical cooligomerization using 2,2'-azobis (2-methyl-propionitrile) as the initiator. The effect of the initiator amount, temperature and reaction time on the yield, softening temperature and molecular weight of CIRM has been established. The structure of the synthesized CIRM has been confirmed by IR and NMR spectroscopy. It is proposed to use CIRM as a polymer component of bitumen-polymeric mixtures (BPS). The effect of CIRM amount, temperature and time on the main characteristics of BPS has been studied.
dc.format.extent379-385
dc.format.pages7
dc.identifier.citationObtaining of coumarone-indene resins based on light fraction of coal tar 3. Coumarone-indene resins with methacrylic fragments / Michael Bratychak, Olena Astakhova, Yuriy Prysiazhnyi, Mariia Shved, Olena Shyshchak, Jacek Namiesnik, Marta Plonska-Brzezinska // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2018. — Vol 12. — No 3. — P. 379–385.
dc.identifier.citationenObtaining of coumarone-indene resins based on light fraction of coal tar 3. Coumarone-indene resins with methacrylic fragments / Michael Bratychak, Olena Astakhova, Yuriy Prysiazhnyi, Mariia Shved, Olena Shyshchak, Jacek Namiesnik, Marta Plonska-Brzezinska // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2018. — Vol 12. — No 3. — P. 379–385.
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/45174
dc.language.isoen
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 3 (12), 2018
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dc.relation.references[22] BratychakM., Ripak O., Namiesnik J. et al.: Chem. Chem. Technol., 2018, 12, 93. https://doi.org/10.23939/chcht12.01.093
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dc.relation.references[24] BS EN 13589:2008. European Standard. Bitumen and bituminous binders. Determination of the tensile properties of modified bitumen by the force ductility method
dc.relation.references[25] BS EN 1426:2000. European Standard. Bitumen and bituminous binders. Methods of tests for petroleum and its products. Determination of needle penetration
dc.relation.references[26] BS EN 1427:2007. European Standard. Bitumen and bituminous binders. Determination of the softening point. Ring and Ball method
dc.relation.references[27] BS EN 13614:2011. European Standard. Bitumen and bituminous binders. Determination of adhesivity of ituminous emulstions by water immersion test
dc.relation.referencesen[1]McNally T. (Ed.): PolymerModified Bitumen. Properties and Characterization. Woodhead Publ., 2011.
dc.relation.referencesen[2] Airey G., J. Mater. Sci., 2004, 39, 951.https://doi.org/10.1023/B:JMSC.0000012927.00747.83
dc.relation.referencesen[3] Fang C., Li T., Zhang Z., Jing D., Polym. Composite., 2008, 29,500. https://doi.org/10.1002/pc.20390
dc.relation.referencesen[4] Pyshyev S., Gunka V., Grytsenko Y., BratychakM., Chem. Chem. Technol., 2016, 10, 631.https://doi.org/10.23939/chcht10.04si.631
dc.relation.referencesen[5] Bahl J., Atheya N., Singh H. et al., Erdoel Kohle, Erdgas, Petrochem., 1993, 46, 22.
dc.relation.referencesen[6] BratychakM., Chervinskyy T., Astakhova O. et al., Chem. Chem. Technol., 2010, 4, 325.
dc.relation.referencesen[7] BratychakM., Grynyshyn O., Astakhova O. et al., Ecolog. Chem. Eng. S, 2010, 17, 309.
dc.relation.referencesen[8] Grynyshyn O., Astakhova O., Chervinskyy T., Chem. Chem. Technol., 2010, 4, 241.
dc.relation.referencesen[9] Strap G., Astakhova O., Lazorko O. et al., Chem. Chem. Technol., 2013, 7, 279.
dc.relation.referencesen[10] BratychakM., Iatsyshyn O., Shyshchak O. et al., Chem. Chem. Technol., 2017, 11, 49. https://doi.org/10.23939/chcht11.01.049
dc.relation.referencesen[11] BratychakM., GaginM., Shyshchak O., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 15.
dc.relation.referencesen[12] BratychakM., GaginM., Shyshchak O., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 21.
dc.relation.referencesen[13] GaginM., BratychakM., Shyshchak O., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 27.
dc.relation.referencesen[14] Chervinskyy T., BratychakM., GaginM., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 1225.
dc.relation.referencesen[15] Skibitskiy V., Grynyshyn O., BratychakM., Waclawek W., Chemia i Inzyneria Ekologiczna, 2004, 11, 41.
dc.relation.referencesen[16] BratychakM., Grynyshyn O., Shyshchak O. et al., Ecolog. Chem. Eng., 2007, 14, 225.
dc.relation.referencesen[17] Grynyshyn O., BratychakM., Krynytskiy V., Donchak V., Chem. Chem. Technol., 2008, 2, 47.
dc.relation.referencesen[18]Wu Y., Li J., Xu J. et al., J. Shanghai Univ. Engl. Ed., 2010,14, 313. https://doi.org/10.1007/s11741-010-0651-3
dc.relation.referencesen[19] Sokolov V., Inden-Kumaronovye Smoly. Metalurgia, Moskva 1978.
dc.relation.referencesen[20] Pyshyev S., Grytsenko Y., Solodkyy S. et al., Chem. Chem. Technol., 2015, 9, 359.
dc.relation.referencesen[21] BratychakM., Astakhova O., Shyshchak O. et al., Chem. Chem. Technol., 2017, 11, 509.https://doi.org/10.23939/chcht11.04.509
dc.relation.referencesen[22] BratychakM., Ripak O., Namiesnik J. et al., Chem. Chem. Technol., 2018, 12, 93. https://doi.org/10.23939/chcht12.01.093
dc.relation.referencesen[23] https://www.chemicalbook.com/ChemicalProductProperty_ EN_CB3415111.htm.
dc.relation.referencesen[24] BS EN 13589:2008. European Standard. Bitumen and bituminous binders. Determination of the tensile properties of modified bitumen by the force ductility method
dc.relation.referencesen[25] BS EN 1426:2000. European Standard. Bitumen and bituminous binders. Methods of tests for petroleum and its products. Determination of needle penetration
dc.relation.referencesen[26] BS EN 1427:2007. European Standard. Bitumen and bituminous binders. Determination of the softening point. Ring and Ball method
dc.relation.referencesen[27] BS EN 13614:2011. European Standard. Bitumen and bituminous binders. Determination of adhesivity of ituminous emulstions by water immersion test
dc.relation.urihttps://doi.org/10.1023/B:JMSC.0000012927.00747.83
dc.relation.urihttps://doi.org/10.1002/pc.20390
dc.relation.urihttps://doi.org/10.23939/chcht10.04si.631
dc.relation.urihttps://doi.org/10.23939/chcht11.01.049
dc.relation.urihttps://doi.org/10.1007/s11741-010-0651-3
dc.relation.urihttps://doi.org/10.23939/chcht11.04.509
dc.relation.urihttps://doi.org/10.23939/chcht12.01.093
dc.relation.urihttps://www.chemicalbook.com/ChemicalProductProperty_
dc.rights.holder© Національний університет „Львівська політехніка“, 2018
dc.rights.holder©Bratychak M., Astakhova O., Prysiazhnyi Y., Shved M., Shyshchak O., Namiesnik J., Plonska-Brzezinska M., 2018
dc.subjectінден-кумаронова смола
dc.subjectкам’яно- вугільна смола
dc.subjectметилметакрилат
dc.subjectазоініціатор
dc.subjectІЧ-спектро- скопія
dc.subjectЯМР-спектроскопія
dc.subjectбітум-полімерна суміш
dc.subjectcoumarone-indene resin
dc.subjectcoal tar
dc.subjectmethyl methacrylate
dc.subjectazoinitiator
dc.subjectIR spectroscopy
dc.subjectNMR spectroscopy
dc.subjectbitumen-polymeric mixture
dc.titleObtaining of coumarone-indene resins based on light fraction of coal tar 3. Coumarone-indene resins with methacrylic fragments
dc.title.alternativeОдержання інден-кумаронових смол з легкої фракції кам‘яно-вугільної смоли 3. Інден-кумаронові смоли з метакрилатними фрагментами
dc.typeArticle

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Chemistry & Chemical Technology. – 2018. – Vol. 12, No. 3