Development of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine

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dc.citation.epage488
dc.citation.issue4
dc.citation.spage482
dc.contributor.affiliationHamadan University of Medical Sciences
dc.contributor.authorPourbakhshi, Yasaman
dc.contributor.authorBahramy, Abdul Rahman
dc.contributor.authorShanha, Farshid Ghorbani
dc.contributor.authorAssari, Mohammad Javad
dc.contributor.authorTajik, Leila
dc.contributor.authorFarhadian, Maryam
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2020-03-03T09:04:14Z
dc.date.available2020-03-03T09:04:14Z
dc.date.created2019-02-28
dc.date.issued2019-02-28
dc.description.abstract2,5-Гександіон (2,5-ГД), основний метаболіт н-гексану, був вилучений із зразків сечі з використанням твердофазної мікроекстракції на основі холодного волокна (CF-HS-SPME) та проаналізований за допомогою газової хроматографії з детектором йонізації полум'я (GC-FID). Важливі параметри для підвищення ефективності сорбції волокна, включаючи об'єм зразка, час екстракції та температуру, оптимізовані за допомогою центрального композиційного плану експерименту. Встановлено оптимальні умови, за яких визначено межу чутливості та відносні стандартні відхилення. Показано, що розроблений метод є швидким, чутливим та простішим у порівнянні із звичайними методами кількісного аналізу 2,5-ГД у зразках сечі.
dc.description.abstract2,5-Hexanedione (2,5-HD), the main metabolite of n-hexane was extracted from urine samples using cold fiber head space solid-phase microextraction (CF-HS-SPME) based on thermoelectric cooling and analyzed with gas chromatography equipped with a flame ionization detector (GC-FID). Important parameters for improved efficiency of fiber sorption including sample volume, extraction time and temperature were optimized using a central composite design. The optimum conditions were determined, under which the detection limit and the relative standard deviations were found. The method was shown to be rapid, sensitive and easier than conventional methods for quantitative analysis of 2,5-HD in urine samples.
dc.format.extent482-488
dc.format.pages7
dc.identifier.citationDevelopment of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine / Yasaman Pourbakhshi, Abdul Rahman Bahramy, Farshid Ghorbani Shanha, Mohammad Javad Assari, Leila Tajik, Maryam Farhadian // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 4. — P. 482–488.
dc.identifier.citationenDevelopment of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine / Yasaman Pourbakhshi, Abdul Rahman Bahramy, Farshid Ghorbani Shanha, Mohammad Javad Assari, Leila Tajik, Maryam Farhadian // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 4. — P. 482–488.
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/46500
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 4 (13), 2019
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dc.relation.urihttps://doi.org/10.1016/S0003-2670(01)01082-0
dc.relation.urihttps://doi.org/10.1134/S1061934815100032
dc.relation.urihttps://doi.org/10.1186/s40201-014-0123-5
dc.relation.urihttps://doi.org/10.1080/00032719.2011.644736
dc.relation.urihttps://doi.org/10.1007/s10661-011-2434-7
dc.relation.urihttps://doi.org/10.1002/jssc.201400262
dc.relation.urihttps://doi.org/10.1002/jssc.201500975
dc.relation.urihttps://doi.org/10.1007/s10661-012-2914-4
dc.relation.urihttps://doi.org/10.1021/ac00097a007
dc.relation.urihttps://doi.org/10.1016/j.chroma.2006.10.092
dc.relation.urihttps://doi.org/10.1021/jf0613942
dc.relation.urihttps://doi.org/10.1002/jssc.200600333
dc.relation.urihttps://doi.org/10.1016/j.aca.2015.10.016
dc.relation.urihttps://doi.org/10.1002/ffj.1809
dc.relation.urihttps://doi.org/10.1016/j.chroma.2008.09.005
dc.relation.urihttps://doi.org/10.1515/pjct-2017-0041
dc.relation.urihttps://doi.org/10.1002/jssc.201201148
dc.relation.urihttps://doi.org/10.1590/S0100-40422007000400009
dc.relation.urihttps://doi.org/10.1016/S1570-0232(02)00036-3
dc.rights.holder© Національний університет „Львівська політехніка“, 2019
dc.rights.holder© Pourbakhshi Y., Bahramy A., Shanha F., Assari M., Tajik L., Farhadian M., 2019
dc.subjectзразки сечі
dc.subject2
dc.subject5-гександіон
dc.subjectхолодне волокно
dc.subjectтвердофазна мікроекстракція
dc.subjectн-гексан
dc.subjecturine samples
dc.subject2
dc.subject5-hexanedione
dc.subjectcold fiber
dc.subjectsolid-phase microextraction
dc.subjectn-hexane
dc.titleDevelopment of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine
dc.title.alternativeТвердофазна мікроекстракція на основі холодного волокна для аналізу 2,5 гександіону в сечі
dc.typeArticle

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Chemistry & Chemical Technology. – 2019. – Vol. 13, No. 4