MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones

Simple item page
dc.citation.epage176
dc.citation.issue2
dc.citation.spage169
dc.citation.volume14
dc.contributor.affiliationScience and Commerce College
dc.contributor.affiliationMilind college of science
dc.contributor.authorKatkar, Santosh Shriram
dc.contributor.authorKategaonkar, Amol Haridas
dc.contributor.authorVidhate, Kaluram N.
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2020-12-30T08:53:34Z
dc.date.available2020-12-30T08:53:34Z
dc.date.created2020-01-24
dc.date.issued2020-01-24
dc.description.abstractМетодом ко-осадження вивчено ряд змішаних оксидів металів Mg-Al, фізико-хімічні властивості яких визначені за допомогою методів РСА, РЕМ, ЕРС, ТЕМ, БЕТ та СО2-ТДС. Розроблено ефективний та простий метод синтезу халконів з використанням різних альдегідів та ацетофенону за допомогою оксиду Mg-Al за умов рефлюксу в етанолі, що забезпечує відмінну продуктивність. Доведено відновлюваність каталізатора, а також здатність MgO до диспергування та підвищення основності, розміру пор і каталітичної активності.
dc.description.abstractWe have studied a series of mixed metal oxides of Mg-Al by a simple co-precipitation technique. Various characterization techniques, including XRD, SEM, EDS, TEM, BET and CO2-TPD were carried out to investigate their physicochemical properties. An efficient and facile protocol has been documented for the synthesis of chalcones using different aldehydes and acetophenone using Mg-Al oxide under reflux conditions in ethanol affording good to excellent yields. Recyclability of a catalyst is a significant feature of this protocol. Moreover, it was proposed that MgO can disperse and increase the basicity, pore size and catalytic activity.
dc.format.extent169-176
dc.format.pages8
dc.identifier.citationKatkar S. S. MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones / Santosh Shriram Katkar, Amol Haridas Kategaonkar, Kaluram N. Vidhate // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 169–176.
dc.identifier.citationenKatkar S. S. MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones / Santosh Shriram Katkar, Amol Haridas Kategaonkar, Kaluram N. Vidhate // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 169–176.
dc.identifier.doidoi.org/10.23939/chcht14.02.169
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/55797
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 2 (14), 2020
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dc.relation.urihttps://doi.org/10.1006/jcat.1996.0246
dc.relation.urihttps://doi.org/10.1016/j.jcat.2006.04.003
dc.relation.urihttps://doi.org/10.1016/S0166-9834(00)80114-1
dc.relation.urihttps://doi.org/10.1016/0926-860X(95)00289-8
dc.relation.urihttps://doi.org/10.1016/S1381-1169(97)00204-5
dc.relation.urihttps://doi.org/10.1021/cr00035a005
dc.relation.urihttps://doi.org/10.1016/S1387-1811(98)00231-5
dc.relation.urihttps://doi.org/10.1006/jcat.2000.3145
dc.relation.urihttps://doi.org/10.1016/S0926-860X(02)00213-2
dc.relation.urihttps://doi.org/10.1021/cm040360b
dc.relation.urihttps://doi.org/10.1021/cm00013a036
dc.relation.urihttps://doi.org/10.1039/b309059k
dc.relation.urihttps://doi.org/10.1016/j.micromeso.2005.04.003
dc.relation.urihttps://doi.org/10.1021/ja994383g
dc.relation.urihttps://doi.org/10.1002/anie.200500663
dc.relation.urihttps://doi.org/10.1006/jcat.1998.2161
dc.relation.urihttps://doi.org/10.1006/jcat.1997.1930
dc.relation.urihttps://doi.org/10.1016/j.apcata.2007.07.038
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dc.rights.holder© Національний університет “Львівська політехніка”, 2020
dc.rights.holder© Katkar S., Kategaonkar A., Vidhate K., 2020
dc.subjectоксид Mg-Al
dc.subjectекологічний каталіз
dc.subjectвідновлюваність
dc.subjectбагатокомпонентна реакція
dc.subjectMg-Al oxide
dc.subjectenvironmental catalysis
dc.subjectrecyclability
dc.subjectmulticomponent reaction
dc.titleMgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones
dc.title.alternativeAl2O3 Нанесений на MgO: новий, ефективний і відновлювальний каталізатор синтезу хальконів
dc.typeArticle

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Chemistry & Chemical Technology. – 2020. – Vol. 14, No. 2