Ionic Liquid-Functionalized Titanomagnetite Nanoparticles as Efficient and Recyclable Catalyst for Green Synthesis of 2,3-Dihydroquinazolin-4(1H)-ones

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dc.citation.epage69
dc.citation.issue1
dc.citation.spage62
dc.contributor.affiliationBu-Ali Sina University
dc.contributor.affiliationTabriz University of Medical Sciences
dc.contributor.authorAzarifar, Davood
dc.contributor.authorBadalkhani, Omolbanin
dc.contributor.authorChehregosha, Morteza
dc.contributor.authorJaymand, Mehdi
dc.coverage.placenameЛьвів
dc.coverage.placenameLviv
dc.date.accessioned2020-12-23T13:23:48Z
dc.date.available2020-12-23T13:23:48Z
dc.date.created2020-01-24
dc.date.issued2020-01-24
dc.description.abstractМетодом ко-осадження синтезовано наночастинки титаномагнетиту (Fe3-xTixO4 NPs) та проведено їх функціоналізацію з використанням 3-триметоксилілпропілхлоридного силанового агента і аспарагінату тетрабутиламонію за допомогою нового однореакторного синтезу з метою одержання Fe3-xTixO4 NPs, модифікованих йонною рідиною. Встановлено, що синтезовані NPs є ефективним і відновлювальним нанокаталізатором однореакторного трикомпонентного синтезу 2,3-дигідрохіназолін-4(1H)-ону без використання розчинників. Показано, що легкість магнітної сепарації та ефективна відновлюваність каталізатора, високі виходи реакцій, малий час реакції, та відсутність розчинників є найважливішими перевагами нового методу. Синтезовані Fe3-xTixO4 NPs можна використовувати як нанокаталізатор у промисловості.
dc.description.abstractIn the present study, titanomagnetite nanoparticles (Fe3-xTixO4 NPs) were synthesized via coprecipitation approach and then functionalized using 3- trimethoxysilylpropyl chloride silan coupling agent followed by tetrabutylammonium asparaginate through a facial and newly one-pot procedure to afford an ionic liquid (IL)-modified Fe3-xTixO4 NPs. The synthesized NPs were examined as potent and recyclable nanocatalysts for one-pot three-component synthesis of 2,3-dihydroquinazolin-4(1H)-ones under solvent-free conditions. Easy magnetic separation and efficient recyclability of the catalyst, excellent yields of the reactions, low reaction times as well as solvent-free conditions are the most important advantages of the present procedure that qualified the fabricated Fe3-xTixO4 NPs as a nanocatalyst for industrial applications.
dc.format.extent62-69
dc.format.pages8
dc.identifier.citationIonic Liquid-Functionalized Titanomagnetite Nanoparticles as Efficient and Recyclable Catalyst for Green Synthesis of 2,3-Dihydroquinazolin-4(1H)-ones / Davood Azarifar, Omolbanin Badalkhani, Morteza Chehregosha, Mehdi Jaymand // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 1. — P. 62–69.
dc.identifier.citationenIonic Liquid-Functionalized Titanomagnetite Nanoparticles as Efficient and Recyclable Catalyst for Green Synthesis of 2,3-Dihydroquinazolin-4(1H)-ones / Davood Azarifar, Omolbanin Badalkhani, Morteza Chehregosha, Mehdi Jaymand // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 1. — P. 62–69.
dc.identifier.doidoi.org/10.23939/chcht14.01.062
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/55759
dc.language.isoen
dc.publisherВидавництво Львівської політехніки
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 1 (14), 2020
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dc.relation.urihttps://doi.org/10.1515/znb-2017-0114
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dc.rights.holder© Національний університет “Львівська політехніка”, 2020
dc.rights.holder© Azarifar D., Badalkhani O., Chehregosha M., Jaymand M., 2020
dc.subjectйонна рідина
dc.subjectнаночастинки титаномагнетиту
dc.subjectнанокаталізатор
dc.subjectзелена хімія
dc.subjectорганічний синтез
dc.subjectionic liquid
dc.subjecttitanomagnetite nanoparticles
dc.subjectnanocatalyst
dc.subjectgreen chemistry
dc.subjectorganic synthesis
dc.titleIonic Liquid-Functionalized Titanomagnetite Nanoparticles as Efficient and Recyclable Catalyst for Green Synthesis of 2,3-Dihydroquinazolin-4(1H)-ones
dc.title.alternativeЙонні рідкофункціоналізовані титаномагнетитні наночастинки як ефективний і відновлювальний каталізатор зеленого синтезу 2,3-дигідрохіназолін-4(1Н)-ону
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Chemistry & Chemical Technology. – 2020. – Vol. 14, No. 1