An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition
dc.citation.epage | 22 | |
dc.citation.issue | 1 | |
dc.citation.spage | 18 | |
dc.contributor.affiliation | G.L.A University | |
dc.contributor.author | Bansal, Shobha | |
dc.contributor.author | Singh, Prabal Pratap | |
dc.coverage.placename | Львів | |
dc.coverage.placename | Lviv | |
dc.date.accessioned | 2020-03-02T10:50:15Z | |
dc.date.available | 2020-03-02T10:50:15Z | |
dc.date.created | 2019-02-28 | |
dc.date.issued | 2019-02-28 | |
dc.description.abstract | Досліджено магнітні наночастинки MgFe2O4 як ефективний каталізатор для синтезу продуктів за реакцією Міхаеля внаслідок оброблення мікрохвилями у відсутності розчинника заміщених халконів і β-нітро стиролів з електронними донорами, такими як малононітрил та етилціаноацетат. Показано, що магнітні наночастинки MgFe2O4 є кращими гетерогенними каталізаторами (10 мол. %) у порівнянні з відомими каталізаторами. Визначено, що за п’ять циклів роботи синтезований каталіза- ор не втрачає каталітичної активності. | |
dc.description.abstract | MgFe2O4 magnetic nanoparticles were used as an efficient catalyst for the synthesis of Michael products by treating substituted chalcones and β-nitro styrenes with electron donar species like malononitrile and ethyl cyanoacetate in solvent free microwave conditions. In this study, we report that MgFe2O4 magnetic nanoparticles were the best heterogeneous catalyst with 10 mol% loading for synthesis of Michael products as compared to several reported catalysts. The reusability of MgFe2O4 nanoparticles was checked for 5 times without appreciable loss of catalytic activity. | |
dc.format.extent | 18-22 | |
dc.format.pages | 5 | |
dc.identifier.citation | Bansal S. An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition / Shobha Bansal, Prabal Pratap Singh // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 1. — P. 18–22. | |
dc.identifier.citationen | Bansal S. An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition / Shobha Bansal, Prabal Pratap Singh // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 1. — P. 18–22. | |
dc.identifier.uri | https://ena.lpnu.ua/handle/ntb/46426 | |
dc.language.iso | en | |
dc.publisher | Видавництво Львівської політехніки | |
dc.publisher | Lviv Politechnic Publishing House | |
dc.relation.ispartof | Chemistry & Chemical Technology, 1 (13), 2019 | |
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dc.relation.referencesen | 1. Gawley R., Synthesis, 1976, 12, 777. https://doi.org/10.1055/s-1976-24200 | |
dc.relation.referencesen | 2. JungM., Tetrahedron, 1976, 32, 3. https://doi.org/10.1016/0040-4020(76)80016-6 | |
dc.relation.referencesen | 3. Peters J: Synthesis, 1979, 5, 321 https://doi.org/10.1055/s-1979-28668 | |
dc.relation.referencesen | 4. Galli C., Marotta E., Right P., Rosini G., J. Org. Chem., 1995, 60, 6624. https://doi.org/10.1021/jo00125a064 | |
dc.relation.referencesen | 5. Hanessian S., Pham V., Org. Lett., 2000, 2, 2975. https://doi.org/10.1021/ol000170g | |
dc.relation.referencesen | 6. Sibi M., Manyem S., Tetrahedron, 2000, 56, 8033. https://doi.org/10.1016/S0040-4020(00)00618-9 | |
dc.relation.referencesen | 7. Ballini R., Bosica G., Fiorini D., Gil M., Synthesis, 2004, 4, 605. https://doi.org/10.1055/s-2004-815948 | |
dc.relation.referencesen | 8. Chandrasekhar S., Rambabu C., Shyamsundar T., Tetrahedron Lett., 2007, 48, 4683. https://doi.org/10.1016/j.tetlet.2007.05.026 | |
dc.relation.referencesen | 9. Tomohiro T., Takuya K., Tsutomu I., Tetrahedron Lett., 2000, 41, 10229. https://doi.org/10.1016/S0040-4039(00)01820-7 | |
dc.relation.referencesen | 10. Spande T., Garraffo H., EdwardsM. et al., J. Am. Chem. Soc., 1992, 114, 3475. https://doi.org/10.1021/ja00035a048 | |
dc.relation.referencesen | 11. Taasu K., Mizutani S., Noguchi M. et al., J. Org. Chem., 2000, 65, 4112. https://doi.org/10.1021/jo000185s | |
dc.relation.referencesen | 12. Bergmann E., Ginsburg D., Pappo R., Org. React. 1959, 10, 179. https://doi.org/10.1002/0471264180.or010.03 | |
dc.relation.referencesen | 13. DaveyW., Gwilt J., J. Chem. Soc., 1957, 1015. https://doi.org/10.1039/jr9570001015 | |
dc.relation.referencesen | 14. Garcia-Raso A., Garcia-Raso J., Campaner B. et al., Synthesis, 1982, 12, 1037. https://doi.org/10.1055/s-1982-30055 | |
dc.relation.referencesen | 15. Ganesh S., Sarkar A., Tetrahedron Lett., 1991, 32, 1085. https://doi.org/10.1016/S0040-4039(00)74494-7 | |
dc.relation.referencesen | 16. Li T-J., Cui Y., Chen G-F. et al., Synth. Commun., 2003, 33, 353. https://doi.org/10.1081/SCC-120015762 | |
dc.relation.referencesen | 17. Ye W-P., Xu J-Y., Tan C-T., Tan C-H., Tetrahedron Lett., 2005, 46, 6875. https://doi.org/10.1016/j.tetlet.2005.08.010 | |
dc.relation.referencesen | 18. ZahouilyM., Bahlaodhuan B., Aadil M. et al., Org. Pro. Res. Develop., 2004, 8, 275. https://doi.org/10.1021/op034161+ | |
dc.relation.referencesen | 19. Ma Y-M., Zhang Y-M., Synth. Commun., 2002, 32, 819. https://doi.org/10.1081/SCC-120002689 | |
dc.relation.referencesen | 20. Meciarova M., Toma S., Chem. Eur. J., 2007, 13, 1268. https://doi.org/10.1002/chem.200600870 | |
dc.relation.referencesen | 21. Gu H., Li J., Qu G. et al., Chirality, 2011, 23, 514. https://doi.org/10.1002/chir.20956 | |
dc.relation.referencesen | 22. Rosnati V., Saba A., Salimbeni A., Tetrahedron Lett., 1981, 22, 167. https://doi.org/10.1016/0040-4039(81)80178-5 | |
dc.relation.referencesen | 23. Toda F., Takumi H., Nagami M., Tanaka K., Hetrocycles, 1998, 47, 469. https://doi.org/10.3987/COM-97-S(N)77 | |
dc.relation.referencesen | 24. Bram G., Sansoulet J., Galons H., MiocqueM., Synth. Commun., 1988, 18, 367. https://doi.org/10.1080/00397918808064000 | |
dc.relation.referencesen | 25. Kim D., Huh S., Kim S., Tetrahedron Lett., 2001, 42, 6299. https://doi.org/10.1016/S0040-4039(01)01237-0 | |
dc.relation.referencesen | 26. Dere R., Pal R., Patil P., SalunkheM., Tetrahedron Lett., 2003, 44, 5351. https://doi.org/10.1016/S0040-4039(03)01198-5 | |
dc.relation.referencesen | 27. Loupy P., Top. Curr. Chem., 1999, 206, 153. https://doi.org/10.1007/3-540-48664-X_7 | |
dc.relation.referencesen | 28. Rao H., Jothilingam S., J. Chem. Sci., 2005, 117, 323. https://doi.org/10.1007/BF02708445 | |
dc.relation.referencesen | 29. Li J., Cui Y., Chen G. et al., Synth. Commun., 2003, 33, 353. https://doi.org/10.1081/SCC-120015762 | |
dc.relation.referencesen | 30. Bansal S., Kumar Y., Pippal P. et al., New J. Chem., 2017, 41, 2668. https://doi.org/10.1039/P.6NJ03701A | |
dc.relation.referencesen | 31. Pippal P., Singh P., Orient. J. Chem., 2017, 33, 1736. https://doi.org/10.13005/ojc/330418 | |
dc.relation.referencesen | 32. SharmaM., Singh P., Bharadwaj P., J. Mol. Catal. A: Chem., 2011, 342, 6. https://doi.org/10.1016/j.molcata.2011.04.016 | |
dc.relation.referencesen | 33. Liang D., Xin X., Gao H. et al., Chem. Res. Chinese Univ., 2009, 25, 169. | |
dc.relation.referencesen | 34. Ying A., Chen X., Wu C. et al., Synth. Commun., 2012, 42, 3455. https://doi.org/10.1080/00397911.2011.584260 | |
dc.relation.referencesen | 35. Guo H., Li J., Qu G. et al., Chirality, 2011, 23, 514. https://doi.org/10.1002/chir.20956 | |
dc.relation.referencesen | 36. Shen Z., Gu D., Yang J., Ji S., Synth. Commun., 2011, 41, 851. https://doi.org/10.1080/00397911003707006 | |
dc.relation.referencesen | 37. Mohammad R., Najmedin A., Elham A., Forogh E., J. Mol. Catal. A, 2008, 292, 44. https://doi.org/10.1016/j.molcata.2008.06.003 | |
dc.relation.referencesen | 38. Shi J., WangM., He L. et al., Chem. Commun., 2009, 4711. https://doi.org/10.1039/b908632c | |
dc.relation.referencesen | 39. Sakthivel V., Kasi P., Ind. J. Chem. B., 2010, 49, 469. | |
dc.relation.uri | https://doi.org/10.1055/s-1976-24200 | |
dc.relation.uri | https://doi.org/10.1016/0040-4020(76)80016-6 | |
dc.relation.uri | https://doi.org/10.1055/s-1979-28668 | |
dc.relation.uri | https://doi.org/10.1021/jo00125a064 | |
dc.relation.uri | https://doi.org/10.1021/ol000170g | |
dc.relation.uri | https://doi.org/10.1016/S0040-4020(00)00618-9 | |
dc.relation.uri | https://doi.org/10.1055/s-2004-815948 | |
dc.relation.uri | https://doi.org/10.1016/j.tetlet.2007.05.026 | |
dc.relation.uri | https://doi.org/10.1016/S0040-4039(00)01820-7 | |
dc.relation.uri | https://doi.org/10.1021/ja00035a048 | |
dc.relation.uri | https://doi.org/10.1021/jo000185s | |
dc.relation.uri | https://doi.org/10.1002/0471264180.or010.03 | |
dc.relation.uri | https://doi.org/10.1039/jr9570001015 | |
dc.relation.uri | https://doi.org/10.1055/s-1982-30055 | |
dc.relation.uri | https://doi.org/10.1016/S0040-4039(00)74494-7 | |
dc.relation.uri | https://doi.org/10.1081/SCC-120015762 | |
dc.relation.uri | https://doi.org/10.1016/j.tetlet.2005.08.010 | |
dc.relation.uri | https://doi.org/10.1021/op034161+ | |
dc.relation.uri | https://doi.org/10.1081/SCC-120002689 | |
dc.relation.uri | https://doi.org/10.1002/chem.200600870 | |
dc.relation.uri | https://doi.org/10.1002/chir.20956 | |
dc.relation.uri | https://doi.org/10.1016/0040-4039(81)80178-5 | |
dc.relation.uri | https://doi.org/10.3987/COM-97-S(N)77 | |
dc.relation.uri | https://doi.org/10.1080/00397918808064000 | |
dc.relation.uri | https://doi.org/10.1016/S0040-4039(01)01237-0 | |
dc.relation.uri | https://doi.org/10.1016/S0040-4039(03)01198-5 | |
dc.relation.uri | https://doi.org/10.1007/3-540-48664-X_7 | |
dc.relation.uri | https://doi.org/10.1007/BF02708445 | |
dc.relation.uri | https://doi.org/10.1039/C6NJ03701A | |
dc.relation.uri | https://doi.org/10.13005/ojc/330418 | |
dc.relation.uri | https://doi.org/10.1016/j.molcata.2011.04.016 | |
dc.relation.uri | https://doi.org/10.1080/00397911.2011.584260 | |
dc.relation.uri | https://doi.org/10.1080/00397911003707006 | |
dc.relation.uri | https://doi.org/10.1016/j.molcata.2008.06.003 | |
dc.relation.uri | https://doi.org/10.1039/b908632c | |
dc.rights.holder | © Національний університет „Львівська політехніка“, 2019 | |
dc.rights.holder | © Bansal S., Singh P., 2019 | |
dc.subject | магнітні наночастинки MgFe2O4 | |
dc.subject | реакція Міхаеля | |
dc.subject | гетерогенний каталізатор | |
dc.subject | MgFe2O4 MNP’s | |
dc.subject | Michael addition | |
dc.subject | heterogeneous catalyst | |
dc.title | An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition | |
dc.title.alternative | Оброблені мікрохвилями у відсутності розчинника магнітні наночастинки MgFe2O4 як ефективний каталізатор реакції Міхаеля | |
dc.type | Article |
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