Synthesis of heterocyclic thioamides and copper(II) coordination compounds based on them

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dc.citation.epage18
dc.citation.issue1
dc.citation.spage11
dc.citation.volume11
dc.contributor.affiliationVinnytsa National Technical University
dc.contributor.authorRanskiy, Anatoliy
dc.contributor.authorDidenko, Natalia
dc.contributor.authorGordienko, Olga
dc.date.accessioned2018-06-20T12:59:11Z
dc.date.available2018-06-20T12:59:11Z
dc.date.created2017-01-20
dc.date.issued2017-01-20
dc.description.abstractМодифікованою реакцією Вільгеродта- Кіндлера синтезовані ариламіди гетарил-2-тіокарбонової кислоти. Отримані сполуки досліджені методами хімічного аналізу, ІЧ- та 1Н ЯМР-спектроскопією. Методами тради- ційного та прямого синтезу на основі бензімідазол-2-N-(4- етоксифенил)карботіоаміда (НL4) отримано кординаційні сполуки загальної формули [Cu(HL4)Cl2]2 · хCH3OH (х = 0, 2). Молекулярна і кристалічна структура комплексу [Cu(HL4)Cl2]2 · 2CH3OH встановлена методом рентгено- структурного аналізу.
dc.description.abstract1Arylamides of hetaryl-2-thiocarboxylic acid were synthesized viaWillgerodt–Kindler modified reaction. The final products were studied by means of chemical analysis, IR- and 1H NMR-spectroscopy. The coordination compounds of the general formula [Cu(HL4)Cl2]2 · ·хCH3OH (х = 0, 2) were obtained via traditional and direct synthesis based on benzimidazol-2-N-(4-ethoxyphenyl) carbothioamide (HL4). Using X-ray analysis the molecular and crystal structures of [Cu(HL4)Cl2]2 · 2CH3OH complex were determined.
dc.format.extent11-18
dc.format.pages8
dc.identifier.citationRanskiy A. Synthesis of heterocyclic thioamides and copper(II) coordination compounds based on them / Anatoliy Ranskiy, Natalia Didenko, Olga Gordienko // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2017. — Vol 11. — No 1. — P. 11–18.
dc.identifier.citationenRanskiy A. Synthesis of heterocyclic thioamides and copper(II) coordination compounds based on them / Anatoliy Ranskiy, Natalia Didenko, Olga Gordienko // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2017. — Vol 11. — No 1. — P. 11–18.
dc.identifier.urihttps://ena.lpnu.ua/handle/ntb/42070
dc.language.isoen
dc.publisherLviv Politechnic Publishing House
dc.relation.ispartofChemistry & Chemical Technology, 1 (11), 2017
dc.relation.references[1] Wang F., LangleyR., Gulten G. et al.: J. Exp. Med., 2007, 204, 73.
dc.relation.references[2] Winogradova V. and Maizus Z.: Kinetika i Kataliz, 1971, 12,1322.
dc.relation.references[3] Ranskiy A., Boichenko S., Gordienko O. et al.: Composytsyini Mastylni Materialy na Osnovi Tioamidiv ta ich Complexnykh spoluk. Vinnytsa VNTU, Vinnytsa 2012.
dc.relation.references[4] Ranskiy A. and Evseeva M.: Sintez, Budova i Reakcii Komplexoutvorennya Aromatychnykh i Heterocyclichnykh Tioamidiv. Vinnytsa VNTU, Vinnytsa 2009.
dc.relation.references[5] Valdez-Rojas J. E., Roios-Guerra H., Ramirez-Sanchez A. et al.: Can. J. Chem., 2012, 90, 567.
dc.relation.references[6] KoketsuM. and Ishihara H.: Curr. Org. Synth., 2007, 4, 15.
dc.relation.references[7] Ranskiy A. and Didenko N. : Chem. Chem. Technol., 2014, 8,317.
dc.relation.references[8] Uraev A., Nivorozhkin A., Korshunov O. et al.: Coordinats. Khimia, 1999, 25, 79.
dc.relation.references[9] Didenko N. and Ranskiy A.: Visnyk Vinnyts. Politechn. Inst.,2012, 3, 182.
dc.relation.references[10] Egorov A., Matynhova S. and Anisimov A.: Appl. Organometall. Chem., 2005, 19, 605.
dc.relation.references[11] Klimova V.: Osnovnye Micrometody Analiza Organicheskykh Soedineniy. Khimiya, Moskva 1975.
dc.relation.references[12] Sheldrick G.: SHELXTL PLUS. PC Version. A system of computer programs for the determination of structure from X-ray diffraction data. Rev. 5.1, 1998.
dc.relation.references[13] Burgi H. and Dunitz J.: Structure Correlation. VCH., Weinheim 1994.
dc.relation.references[14] Orpen G., Brammer L., Allen F. H. et al.: J. Chem. Dalton Trans., 1989, 12, S1.
dc.relation.referencesen[1] Wang F., LangleyR., Gulten G. et al., J. Exp. Med., 2007, 204, 73.
dc.relation.referencesen[2] Winogradova V. and Maizus Z., Kinetika i Kataliz, 1971, 12,1322.
dc.relation.referencesen[3] Ranskiy A., Boichenko S., Gordienko O. et al., Composytsyini Mastylni Materialy na Osnovi Tioamidiv ta ich Complexnykh spoluk. Vinnytsa VNTU, Vinnytsa 2012.
dc.relation.referencesen[4] Ranskiy A. and Evseeva M., Sintez, Budova i Reakcii Komplexoutvorennya Aromatychnykh i Heterocyclichnykh Tioamidiv. Vinnytsa VNTU, Vinnytsa 2009.
dc.relation.referencesen[5] Valdez-Rojas J. E., Roios-Guerra H., Ramirez-Sanchez A. et al., Can. J. Chem., 2012, 90, 567.
dc.relation.referencesen[6] KoketsuM. and Ishihara H., Curr. Org. Synth., 2007, 4, 15.
dc.relation.referencesen[7] Ranskiy A. and Didenko N. : Chem. Chem. Technol., 2014, 8,317.
dc.relation.referencesen[8] Uraev A., Nivorozhkin A., Korshunov O. et al., Coordinats. Khimia, 1999, 25, 79.
dc.relation.referencesen[9] Didenko N. and Ranskiy A., Visnyk Vinnyts. Politechn. Inst.,2012, 3, 182.
dc.relation.referencesen[10] Egorov A., Matynhova S. and Anisimov A., Appl. Organometall. Chem., 2005, 19, 605.
dc.relation.referencesen[11] Klimova V., Osnovnye Micrometody Analiza Organicheskykh Soedineniy. Khimiya, Moskva 1975.
dc.relation.referencesen[12] Sheldrick G., SHELXTL PLUS. PC Version. A system of computer programs for the determination of structure from X-ray diffraction data. Rev. 5.1, 1998.
dc.relation.referencesen[13] Burgi H. and Dunitz J., Structure Correlation. VCH., Weinheim 1994.
dc.relation.referencesen[14] Orpen G., Brammer L., Allen F. H. et al., J. Chem. Dalton Trans., 1989, 12, S1.
dc.rights.holder© Національний університет „Львівська політехніка“, 2017
dc.rights.holder© Ranskiy A., Didenko N., Gordienko O., 2017
dc.subjectгетероциклічні тіоаміди
dc.subjectбіядерні комплекси купруму(ІІ)
dc.subjectрентгеноструктурний аналіз
dc.subjectheterocyclic thioamide
dc.subjectcopper(II) binuclear complex
dc.subjectX-ray analysis
dc.titleSynthesis of heterocyclic thioamides and copper(II) coordination compounds based on them
dc.title.alternativeСинтез гетероциклічних тіоамідів та координаційних сполук купруму(II) на їх основі
dc.typeArticle

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Chemistry & Chemical Technology. – 2017. – Vol. 11, No. 1